TA15/TaZrNb multi-element alloy prepared via diffusion bonding: Tensile-strength model and performance of a representative volume element embedded with a sphere

In this study, to meet the development and application requirements for high-strength and high-toughness energetic structural materials, a representative volume element of a TA15 matrix embedded with a TaZrNb sphere was designed and fabricated via diffusion bonding. The mechanisms of the microstructural evolution of the TaZrNb/TA15 interface were investigated via SEM, EBSD, EDS, and XRD. Interface mechanical property tests and in-situ tensile tests were conducted on the sphere-containing structure, and an equivalent tensile-strength model was established for the structure. The results revealed that the TA15 titanium alloy and joint had high density and no pores or cracks. The thickness of the planar joint was approximately 50–60 μm. The average tensile and shear strengths were 767 MPa and 608 MPa, respectively. The thickness of the spherical joint was approximately 60 μm. The Zr and Nb elements in the joint diffused uniformly and formed strong bonds with Ti without forming intermetallic compounds. The interface exhibited submicron grain refinement and a concave–convex interlocking structure. The tensile fracture surface primarily exhibited intergranular fracture combined with some transgranular fracture, which constituted a quasi-brittle fracture mode. The shear fracture surface exhibited brittle fracture with regular arrangements of furrows. Internal fracture occurred along the spherical interface, as revealed by advanced in-situ X-ray microcomputed tomography. The experimental results agreed well with the theoretical predictions, indicating that the high-strength interface contributes to the overall strength and toughness of the sphere-containing structure. • High-strength mechanical properties of the interface of the TA15/TaZrNb MEA composite fabricated via diffusion bonding. • Investigation on the fracture mechanisms of the RVE embedded with a sphere by in-situ μCT tensile tests. • A tensile-strength equivalent model for the RVE embedded with a sphere is established. • The concave–convex interlocking structure at the interface plays a crucial role in resisting failure.

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Journal
Defence Technology
Published
2025-03-27
DOI
https://doi.org/10.1016/j.dt.2025.03.018
Primary Topic
Intermetallics and Advanced Alloy Properties
Type
article
Field-Weighted Citation Impact
0.00

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article

TA15/TaZrNb multi-element alloy prepared via diffusion bonding: Tensile-strength model and performance of a representative volume element embedded with a sphere

Aiguo Pi, Lida Che, Chuan Ting Wang, Fenglei Huang et al.
Defence Technology
Intermetallics and Advanced Alloy Properties
article

TA15/TaZrNb multi-element alloy prepared via diffusion bonding: Tensile-strength model and performance of a representative volume element embedded with a sphere

Aiguo Pi, Lida Che, Chuan Ting Wang, Fenglei Huang, Fan Rui-jun, Pengjie Zhang, Wei Chen
article en

Abstract

In this study, to meet the development and application requirements for high-strength and high-toughness energetic structural materials, a representative volume element of a TA15 matrix embedded with a TaZrNb sphere was designed and fabricated via diffusion bonding. The mechanisms of the microstructural evolution of the TaZrNb/TA15 interface were investigated via SEM, EBSD, EDS, and XRD. Interface mechanical property tests and in-situ tensile tests were conducted on the sphere-containing structure, and an equivalent tensile-strength model was established for the structure. The results revealed that the TA15 titanium alloy and joint had high density and no pores or cracks. The thickness of the planar joint was approximately 50–60 μm. The average tensile and shear strengths were 767 MPa and 608 MPa, respectively. The thickness of the spherical joint was approximately 60 μm. The Zr and Nb elements in the joint diffused uniformly and formed strong bonds with Ti without forming intermetallic compounds. The interface exhibited submicron grain refinement and a concave–convex interlocking structure. The tensile fracture surface primarily exhibited intergranular fracture combined with some transgranular fracture, which constituted a quasi-brittle fracture mode. The shear fracture surface exhibited brittle fracture with regular arrangements of furrows. Internal fracture occurred along the spherical interface, as revealed by advanced in-situ X-ray microcomputed tomography. The experimental results agreed well with the theoretical predictions, indicating that the high-strength interface contributes to the overall strength and toughness of the sphere-containing structure. • High-strength mechanical properties of the interface of the TA15/TaZrNb MEA composite fabricated via diffusion bonding. • Investigation on the fracture mechanisms of the RVE embedded with a sphere by in-situ μCT tensile tests. • A tensile-strength equivalent model for the RVE embedded with a sphere is established. • The concave–convex interlocking structure at the interface plays a crucial role in resisting failure.

Defence TechnologyVol. 50
Beijing Institute of Technology (CN), Nanjing University of Science and Technology (CN), Advanced Technology & Materials (China) (CN)
National Natural Science Foundation of China
Openalex Percentile: Top 94%
Intermetallics and Advanced Alloy Properties
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