Evaluation of surface treatment methods and their influence on the mechanical performance of hybrid metal-composite laminates

Abstract Fiber metal laminates (FMLs), which fuse the strengths of alloys and fiber-reinforced composites, find application in the aerospace and automobile sectors. Despite the benefits, functional performance depends on the quality of the bonding strength at the metal-composite interface. Therefore, in the present study, effect of mechanical abrasion (MA), nitric acid etching (NI), P2 etching (P2), sulfuric acid anodizing (SA), and electric discharge texturing (ED) surface treatments methods was evaluated by considering the surface morphology, roughness, wettability, and surface energy. Furthermore, the impact of surface treatment methods on the tensile and flexural behavior of Carbon Reinforced Aluminum Laminate (CARALL) fabricated using the treated aluminum substrate was studied and compared with untreated laminates. The results showed that all treatment methods increased the surface roughness of the aluminum substrate. MA and ED treatments imparted higher surface roughness (0.95 and 1.85 μm), with the surface displaying hydrophobic behavior, while chemical and SA treatments increased the surface energy (39.1 MJ m −2 , 45.2 MJ m −2 , and 60.1 MJ m −2 ) and produced surfaces exhibiting hydrophilic behavior. Surface treatments helped improve the ultimate tensile strength of CARALL laminates. The highest improvement, 61%, was achieved using SA treatment (921.43 MPa), while MA resulted in a modest 38% improvement (789.82 MPa). SA treatment increased the elastic modulus and toughness by 188% and 82% in comparison to the untreated specimens. A similar increase in flexural strength was noted, with a 35% increase in the case of MA and a maximum 104% increment from SA, as against untreated ones. Flexural modulus and toughness of 88.05 GPa and 32.39 MJ m −3 was attained with the help of SA treatment. Delamination was observed during the plastic deformation stage under the tensile loading conditions. However, delamination occurred during the end stages of failure under flexural loading, indicating a higher delamination resistance offering by CARALL with flexural loading conditions.

Authors

Institutions

Publication Details

Journal
Materials Research Express
Published
2025-03-26
DOI
https://doi.org/10.1088/2053-1591/adc543
Primary Topic
Material Properties and Applications
Type
article
Field-Weighted Citation Impact
0.00
Controls
|||
ALL TIME
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
article

Evaluation of surface treatment methods and their influence on the mechanical performance of hybrid metal-composite laminates

Gururaj Bolar, B. Satish Shenoy, Madhusudhan Balkundhi
Materials Research Express
Material Properties and Applications
article

Evaluation of surface treatment methods and their influence on the mechanical performance of hybrid metal-composite laminates

Gururaj Bolar, B. Satish Shenoy, Madhusudhan Balkundhi
article en

Abstract

Abstract Fiber metal laminates (FMLs), which fuse the strengths of alloys and fiber-reinforced composites, find application in the aerospace and automobile sectors. Despite the benefits, functional performance depends on the quality of the bonding strength at the metal-composite interface. Therefore, in the present study, effect of mechanical abrasion (MA), nitric acid etching (NI), P2 etching (P2), sulfuric acid anodizing (SA), and electric discharge texturing (ED) surface treatments methods was evaluated by considering the surface morphology, roughness, wettability, and surface energy. Furthermore, the impact of surface treatment methods on the tensile and flexural behavior of Carbon Reinforced Aluminum Laminate (CARALL) fabricated using the treated aluminum substrate was studied and compared with untreated laminates. The results showed that all treatment methods increased the surface roughness of the aluminum substrate. MA and ED treatments imparted higher surface roughness (0.95 and 1.85 μm), with the surface displaying hydrophobic behavior, while chemical and SA treatments increased the surface energy (39.1 MJ m −2 , 45.2 MJ m −2 , and 60.1 MJ m −2 ) and produced surfaces exhibiting hydrophilic behavior. Surface treatments helped improve the ultimate tensile strength of CARALL laminates. The highest improvement, 61%, was achieved using SA treatment (921.43 MPa), while MA resulted in a modest 38% improvement (789.82 MPa). SA treatment increased the elastic modulus and toughness by 188% and 82% in comparison to the untreated specimens. A similar increase in flexural strength was noted, with a 35% increase in the case of MA and a maximum 104% increment from SA, as against untreated ones. Flexural modulus and toughness of 88.05 GPa and 32.39 MJ m −3 was attained with the help of SA treatment. Delamination was observed during the plastic deformation stage under the tensile loading conditions. However, delamination occurred during the end stages of failure under flexural loading, indicating a higher delamination resistance offering by CARALL with flexural loading conditions.

Materials Research ExpressVol. 12(4)
Manipal Academy of Higher Education (IN)
Openalex Percentile: Top 92%
Material Properties and Applications
AI Navigator

Ask Laika to Summarize, Analyze, and Connect papers live on the map.

Summarize Papers & Methodologies

Extract key findings, datasets, and comparative methods across publications.

Benchmark Rankings & Visual Analytics

Rank top research institutions, authors, funders, topics, and journals by Field-Weighted Citation Impact (FWCI) and paper volume with instant charts.

Connect Distant Disciplines

Bridge topological clusters on the map to find hidden collaborative intersections.