Synthesis and Characterization of Some New Bis (1,3-selenazole) from Bis-Selenocarboxamide

The synthesis of new bis (1,3-selenazoles) was achieved by subjecting primary bis aryl-selenocarboxylic amides to cyclization with α-bromoketones. The methodical preparation of bis (1,3-selenazoles) was achieved by the primary bis selenoamides with α-halo ketones. Bis selenoamides were gained from the reaction of NaHSe with aryl nitrile. The resulting bis (1,3-selenazoles) has been characterized by different spectroscopic methods; such as 1H ,13C NMR, IR, and mass spectroscopic data to prove the structural formula of the prepared compounds.

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Publication Details

Journal
Iraqi Journal of Natural Sciences and Nanotechnology
Published
2025-03-21
DOI
https://doi.org/10.47758/ijnsn.v6i1.132
Primary Topic
Organoselenium and organotellurium chemistry
Type
article
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article

Synthesis and Characterization of Some New Bis (1,3-selenazole) from Bis-Selenocarboxamide

Ali Jameel Hameed, Anwar Talib Abdulwahid
Iraqi Journal of Natural Sciences and Nanotechnology
Organoselenium and organotellurium chemistry
article

Synthesis and Characterization of Some New Bis (1,3-selenazole) from Bis-Selenocarboxamide

Ali Jameel Hameed, Anwar Talib Abdulwahid
article en

Abstract

The synthesis of new bis (1,3-selenazoles) was achieved by subjecting primary bis aryl-selenocarboxylic amides to cyclization with α-bromoketones. The methodical preparation of bis (1,3-selenazoles) was achieved by the primary bis selenoamides with α-halo ketones. Bis selenoamides were gained from the reaction of NaHSe with aryl nitrile. The resulting bis (1,3-selenazoles) has been characterized by different spectroscopic methods; such as 1H ,13C NMR, IR, and mass spectroscopic data to prove the structural formula of the prepared compounds.

Iraqi Journal of Natural Sciences and NanotechnologyVol. 6(1)
University of Basrah (IQ)
Clean water and sanitation
Openalex Percentile: Top 94%
Organoselenium and organotellurium chemistry
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