Microstructure and mechanical properties of multidirectionally forged Al alloy 1570С subjected to cryogenic rolling

The effect of cryogenic rolling at -196°C up to 90% reduction on the microstructure and static strength of a 1570C alloy (Al-5.0Mg-0.18Mn-0.2Sc-0.08Zr-0.01Fe-0.01Si wt%), pre-processed by multidirectional isothermal forging (MIF) at 325°C to a total strain of about 12, is investigated. MIF of the homogenized ingot allowed to obtain a near-homogeneous (ultra)fine grained (UFG) structure with a grain size of 2.3 μm, leveled Mg in solid solution and a uniform distribution of second phases, which ensured subsequent rolling without cracking. Rolling transformed the forged structure into a pancaked (flattened) UFG high work-hardened structure with a halved fraction of high-angle boundaries, characterized by a dislocation density of 10 15 m -2 and a partially developed nano-sized crystallite structure with a coherent domain size of 15 nm. These structural changes resulted in significant improvements in room temperature tensile strength compared to the initial homogenized/forged conditions: yield strength increased from 245/235 to 590 MPa and ultimate tensile strength increased from 355/365 to 620 MPa, while elongation decreased from 26/37 to 9%. The increase in strength with reduced ductility is attributed to the superposition of grain boundary and dislocation strengthening mechanisms amid dispersion strengthening. Therewith, cryogenic rolling promotes uniform dislocation structures and a homogeneous distribution of Al 3 (Sc,Zr) precipitates, which interact with the dislocations to maintain relatively high ductility even in a highly deformed state.

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Publication Details

Journal
International Journal of Lightweight Materials and Manufacture
Published
2025-03-01
DOI
https://doi.org/10.1016/j.ijlmm.2025.03.005
Primary Topic
Metallurgy and Material Forming
Type
article
Field-Weighted Citation Impact
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article

Microstructure and mechanical properties of multidirectionally forged Al alloy 1570С subjected to cryogenic rolling

Rinat Zagitov, O. E. Latypova, S. V. Krymskiy, М. В. Маркушев et al.
International Journal of Lightweight Materials and Manufacture
Metallurgy and Material Forming
article

Microstructure and mechanical properties of multidirectionally forged Al alloy 1570С subjected to cryogenic rolling

Rinat Zagitov, O. E. Latypova, S. V. Krymskiy, М. В. Маркушев, Oleg Sitdikov, Е. В. Автократова
article en

Abstract

The effect of cryogenic rolling at -196°C up to 90% reduction on the microstructure and static strength of a 1570C alloy (Al-5.0Mg-0.18Mn-0.2Sc-0.08Zr-0.01Fe-0.01Si wt%), pre-processed by multidirectional isothermal forging (MIF) at 325°C to a total strain of about 12, is investigated. MIF of the homogenized ingot allowed to obtain a near-homogeneous (ultra)fine grained (UFG) structure with a grain size of 2.3 μm, leveled Mg in solid solution and a uniform distribution of second phases, which ensured subsequent rolling without cracking. Rolling transformed the forged structure into a pancaked (flattened) UFG high work-hardened structure with a halved fraction of high-angle boundaries, characterized by a dislocation density of 10 15 m -2 and a partially developed nano-sized crystallite structure with a coherent domain size of 15 nm. These structural changes resulted in significant improvements in room temperature tensile strength compared to the initial homogenized/forged conditions: yield strength increased from 245/235 to 590 MPa and ultimate tensile strength increased from 355/365 to 620 MPa, while elongation decreased from 26/37 to 9%. The increase in strength with reduced ductility is attributed to the superposition of grain boundary and dislocation strengthening mechanisms amid dispersion strengthening. Therewith, cryogenic rolling promotes uniform dislocation structures and a homogeneous distribution of Al 3 (Sc,Zr) precipitates, which interact with the dislocations to maintain relatively high ductility even in a highly deformed state.

International Journal of Lightweight Materials and Manufacture
Institute of Metal Superplasticity Problems (RU)
Russian Science Foundation
Openalex Percentile: Top 94%
Metallurgy and Material Forming
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Microstructure and mechanical properties of multidirectionally forged Al alloy 1570С subjected to cryogenic rolling — Rinat Zagitov, O. E. Latypova, et al. · International Journal of Lightweight Materials and Manufacture (2025) | TGRS Research Map | TGRS