Synthesis and Characterization of Metal Complexes derived from 4-Methyl-2-Oxo-2H-Chromen-7-yl-Acetate.

A new ligand AMC (7-acetoxy-4-methyl coumarin or 4-methyl-2-oxo-2H-chromen-7-yl-acetate) is prepared from the condensation of resorcinol, ethyl acetoacetate and acetic anhydride. A new metal chelates derived from 4-methyl-2-oxo-2H-chromen-7-yl-acetate with Ni (II) and Cu (II) ions. The metal chelates was prepared and characterized by IR, NMR, TGA-DTA, XRD, Elemental analysis and molar conductance measurements. The AMC ligand and their metal chelates have been tested for their antimicrobial activity using Broth Dilution Method and the results were discussed.

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Publication Details

Journal
African Journal of Biomedical Research
Published
2024-12-30
DOI
https://doi.org/10.53555/ajbr.v27i4s.7159
Primary Topic
Synthesis of Organic Compounds
Type
article
Field-Weighted Citation Impact
0.00

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article

Synthesis and Characterization of Metal Complexes derived from 4-Methyl-2-Oxo-2H-Chromen-7-yl-Acetate.

Niteen B. Tarate
African Journal of Biomedical Research
Synthesis of Organic Compounds
article

Synthesis and Characterization of Metal Complexes derived from 4-Methyl-2-Oxo-2H-Chromen-7-yl-Acetate.

Niteen B. Tarate
article en

Abstract

A new ligand AMC (7-acetoxy-4-methyl coumarin or 4-methyl-2-oxo-2H-chromen-7-yl-acetate) is prepared from the condensation of resorcinol, ethyl acetoacetate and acetic anhydride. A new metal chelates derived from 4-methyl-2-oxo-2H-chromen-7-yl-acetate with Ni (II) and Cu (II) ions. The metal chelates was prepared and characterized by IR, NMR, TGA-DTA, XRD, Elemental analysis and molar conductance measurements. The AMC ligand and their metal chelates have been tested for their antimicrobial activity using Broth Dilution Method and the results were discussed.

African Journal of Biomedical Research
Savitribai Phule Pune University
Openalex Percentile: Top 74%
Synthesis of Organic Compounds
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