Effect of Filament Pre-Drying on the Microstructure and Porosity of 3D Printed PLA

This paper explored the effect of filament pre-drying before 3D printing. A comparison between the undried and pre-dried 3D printed PLA was evaluated in terms of porosity, microstructure, and polymeric chain bonding. Three conditions were examined: a new PLA as a reference, used PLA filament stored in a vacuumed bag with 50g desiccant, and used PLA exposed to humidity for 48h, 96h, and 150h. The parameter setting for drying and 3D printing was constant for all conditions. As a result, pre-drying the filament resulted in a less porous microstructure, shorter interlayer gap, and better interlayer adhesion. The pre-drying method offers a better microstructure than undried filament. The density of the pre-dried sample was increased as the porosity decreased due to the improvement in the mass flow rate upon the extrusion process. Lastly, the FTIR analysis shows that the pre-dried filament exhibits an O-H molecule free from the O-H region broad peak, which shows no or almost no presence of water (H2O).

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Publication Details

Journal
Journal of Advanced Research in Micro and Nano Engieering
Published
2024-10-31
DOI
https://doi.org/10.37934/armne.24.1.8594
Citations
1
Primary Topic
biodegradable polymer synthesis and properties
Type
article
Field-Weighted Citation Impact
0.17

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article

Effect of Filament Pre-Drying on the Microstructure and Porosity of 3D Printed PLA

Shajahan Maidin, Rahimah Abdul Hamid, Teruaki Ito, Siti Hidayah Husni et al.
1 citations
Journal of Advanced Research in Micro and Nano Engieering
biodegradable polymer synthesis and properties
0.17
article

Effect of Filament Pre-Drying on the Microstructure and Porosity of 3D Printed PLA

Shajahan Maidin, Rahimah Abdul Hamid, Teruaki Ito, Siti Hidayah Husni, Madihah Maharof
article en
1 citations

Abstract

This paper explored the effect of filament pre-drying before 3D printing. A comparison between the undried and pre-dried 3D printed PLA was evaluated in terms of porosity, microstructure, and polymeric chain bonding. Three conditions were examined: a new PLA as a reference, used PLA filament stored in a vacuumed bag with 50g desiccant, and used PLA exposed to humidity for 48h, 96h, and 150h. The parameter setting for drying and 3D printing was constant for all conditions. As a result, pre-drying the filament resulted in a less porous microstructure, shorter interlayer gap, and better interlayer adhesion. The pre-drying method offers a better microstructure than undried filament. The density of the pre-dried sample was increased as the porosity decreased due to the improvement in the mass flow rate upon the extrusion process. Lastly, the FTIR analysis shows that the pre-dried filament exhibits an O-H molecule free from the O-H region broad peak, which shows no or almost no presence of water (H2O).

Journal of Advanced Research in Micro and Nano EngieeringVol. 24(1)
Okayama Prefectural University (JP), Technical University of Malaysia Malacca (MY), Islamic University of Technology (BD), SEGi University (MY)
Universiti Teknikal Malaysia Melaka
Openalex Percentile: Top 48%
biodegradable polymer synthesis and properties
0.17
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