Fabrication and Mechanical Properties of Textured Ti<sub>3</sub>SiC<sub>2</sub> by Slip Casting in a Strong Magnetic Field Followed by Spark Plasma Sintering
Ti3SiC2 with a nacre-like microstructure was fabricated by slip casting in a strong magnetic field followed by spark plasma sintering (SPS). To determine the effect of the grain size and texture on the mechanical properties, two textured and non-textured Ti3SiC2 ceramics with different grain sizes were prepared with the different initial particle size and SPS sintering temperature. A powder with relatively large plate-like Ti3SiC2 particles was fabricated by the templated-grain growth method. Increasing the grain size increased the fracture toughness of the textured Ti3SiC2 ceramics but decreased the three-point bending strength. The three-point bending strength and fracture toughness of the textured Ti3SiC2 with the large grain size were 812 MPa and 7.3 MPa・m1/2, and those with the small grain size were 1045 MPa and 5.6 MPa・m1/2, respectively. Furthermore, catastrophic failure of the textured Ti3SiC2 ceramics after the fracture toughness test was prevented, similarly to in fiber-reinforced ceramics.
Authors
- Yoshio Sakka (ORCID: https://orcid.org/0000-0001-8357-5843)
- Takamasa Ishigaki (ORCID: https://orcid.org/0000-0002-7373-5708)
- T. Suzuki (ORCID: https://orcid.org/0000-0001-9458-6863)
- Kimitoshi Sato (ORCID: https://orcid.org/0000-0002-2050-5802)
- Koji Morita (ORCID: https://orcid.org/0000-0002-1808-5167)
- Hiroto Hirano
Institutions
- Hosei University (JP)
- National Institute for Materials Science (JP)
Publication Details
- Journal
- Journal of the Japan Society of Powder and Powder Metallurgy
- Published
- 2025-03-14
- DOI
- https://doi.org/10.2497/jjspm.16b-t5-06
- Primary Topic
- MXene and MAX Phase Materials
- Type
- article
- Field-Weighted Citation Impact
- 0.00
Funders
- Japan Society for the Promotion of Science