Fabrication and Mechanical Properties of Textured Ti<sub>3</sub>SiC<sub>2</sub> by Slip Casting in a Strong Magnetic Field Followed by Spark Plasma Sintering

Ti3SiC2 with a nacre-like microstructure was fabricated by slip casting in a strong magnetic field followed by spark plasma sintering (SPS). To determine the effect of the grain size and texture on the mechanical properties, two textured and non-textured Ti3SiC2 ceramics with different grain sizes were prepared with the different initial particle size and SPS sintering temperature. A powder with relatively large plate-like Ti3SiC2 particles was fabricated by the templated-grain growth method. Increasing the grain size increased the fracture toughness of the textured Ti3SiC2 ceramics but decreased the three-point bending strength. The three-point bending strength and fracture toughness of the textured Ti3SiC2 with the large grain size were 812 MPa and 7.3 MPa・m1/2, and those with the small grain size were 1045 MPa and 5.6 MPa・m1/2, respectively. Furthermore, catastrophic failure of the textured Ti3SiC2 ceramics after the fracture toughness test was prevented, similarly to in fiber-reinforced ceramics.

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Publication Details

Journal
Journal of the Japan Society of Powder and Powder Metallurgy
Published
2025-03-14
DOI
https://doi.org/10.2497/jjspm.16b-t5-06
Primary Topic
MXene and MAX Phase Materials
Type
article
Field-Weighted Citation Impact
0.00

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article

Fabrication and Mechanical Properties of Textured Ti3SiC2 by Slip Casting in a Strong Magnetic Field Followed by Spark Plasma Sintering

Yoshio Sakka, Takamasa Ishigaki, T. Suzuki, Kimitoshi Sato et al.
2 links
Journal of the Japan Society of Powder and Powder Metallurgy
MXene and MAX Phase Materials
article

Fabrication and Mechanical Properties of Textured Ti3SiC2 by Slip Casting in a Strong Magnetic Field Followed by Spark Plasma Sintering

Yoshio Sakka, Takamasa Ishigaki, T. Suzuki, Kimitoshi Sato, Koji Morita, Hiroto Hirano
article en

Abstract

Ti3SiC2 with a nacre-like microstructure was fabricated by slip casting in a strong magnetic field followed by spark plasma sintering (SPS). To determine the effect of the grain size and texture on the mechanical properties, two textured and non-textured Ti3SiC2 ceramics with different grain sizes were prepared with the different initial particle size and SPS sintering temperature. A powder with relatively large plate-like Ti3SiC2 particles was fabricated by the templated-grain growth method. Increasing the grain size increased the fracture toughness of the textured Ti3SiC2 ceramics but decreased the three-point bending strength. The three-point bending strength and fracture toughness of the textured Ti3SiC2 with the large grain size were 812 MPa and 7.3 MPa・m1/2, and those with the small grain size were 1045 MPa and 5.6 MPa・m1/2, respectively. Furthermore, catastrophic failure of the textured Ti3SiC2 ceramics after the fracture toughness test was prevented, similarly to in fiber-reinforced ceramics.

Journal of the Japan Society of Powder and Powder MetallurgyVol. 72(Supplement)
Hosei University (JP), National Institute for Materials Science (JP)
Japan Society for the Promotion of Science
Openalex Percentile: Top 97%
MXene and MAX Phase Materials
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