Effect of Overheating Temperature on Microstructure and Hardness of HP40 Nb Alloy: Analysis by ANOVA

In this study, the influence of short-term overheating on the microstructure and hardness of tube segments made of centrifugally cast austenitic alloy HP40 Nb that were exposed to high temperatures in a stream of hydrocarbons and water vapor, at low pressure for more than 100,000 hours has been studied. Samples were heated up to 1223, 1323, and 1423 K under air at different time intervals from 30 to 480 min, respectively. Microstructural investigation and chemical analysis of as-cast and heat-treated specimens were performed by scanning electron microscopy and energy dispersive spectroscopy. The results showed significant differences in microstructure and hardness after short-term overheating. The results obtained were analyzed using regression analysis and ANOVA methods. The highest hardness of 203.85 HV10 was obtained after overheating at 1223 K for 480 min. The test results were analyzed using regression analysis and ANOVA test. ANOVA test confirmed the results with a 71.82 % model representativeness for hardness. This paper provides insights into the effects of short-term overheating on the mechanical properties of HP40 Nb grade steel after long-term operating conditions at high temperatures, which may be significant for improving performance and predicting the remaining life of the tubes made of HP40 Nb.

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Journal
Materials Science
Published
2025-03-05
DOI
https://doi.org/10.5755/j02.ms.37697
Primary Topic
Metallurgy and Material Forming
Type
article
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article

Effect of Overheating Temperature on Microstructure and Hardness of HP40 Nb Alloy: Analysis by ANOVA

Milica Timotijević, Olivera Erić Cekić, Mića Đurđev, Aleksandar Devečerski et al.
Materials Science
Metallurgy and Material Forming
article

Effect of Overheating Temperature on Microstructure and Hardness of HP40 Nb Alloy: Analysis by ANOVA

Milica Timotijević, Olivera Erić Cekić, Mića Đurđev, Aleksandar Devečerski, Dragan Rajnović, Petar Janjatović
article en

Abstract

In this study, the influence of short-term overheating on the microstructure and hardness of tube segments made of centrifugally cast austenitic alloy HP40 Nb that were exposed to high temperatures in a stream of hydrocarbons and water vapor, at low pressure for more than 100,000 hours has been studied. Samples were heated up to 1223, 1323, and 1423 K under air at different time intervals from 30 to 480 min, respectively. Microstructural investigation and chemical analysis of as-cast and heat-treated specimens were performed by scanning electron microscopy and energy dispersive spectroscopy. The results showed significant differences in microstructure and hardness after short-term overheating. The results obtained were analyzed using regression analysis and ANOVA methods. The highest hardness of 203.85 HV10 was obtained after overheating at 1223 K for 480 min. The test results were analyzed using regression analysis and ANOVA test. ANOVA test confirmed the results with a 71.82 % model representativeness for hardness. This paper provides insights into the effects of short-term overheating on the mechanical properties of HP40 Nb grade steel after long-term operating conditions at high temperatures, which may be significant for improving performance and predicting the remaining life of the tubes made of HP40 Nb.

Materials ScienceVol. 32(2)
University of Kragujevac (RS), University of Novi Sad (RS), University of Belgrade (RS)
Openalex Percentile: Top 96%
Metallurgy and Material Forming
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