Grain structure control of a novel titanium alloy during laser powder bed fusion by processing

The characteristic of rapid solidification in additive manufacturing can address the challenge of brittle fracture caused by the segregation of O and Fe atoms in titanium alloys. This paper studied the effects of process parameters of L-PBF and heat treatment on the microstructure and mechanical properties of Ti-0.4O-3Fe alloy. The research indicated that equiaxed prior-β grains were obtained at a low energy density (91J/mm 3 ), while columnar prior-β grains were obtained at a high energy density (164J/mm 3 ). Meanwhile, the α' martensite of less than 1 μm in size and GB-α were distributed in the intracrystalline and grain boundaries of the prior-β grains, respectively. The as-fabricated state of the L-PBF process exhibited high strength but compromised ductility. After annealing at 600°C for 2 hours, excellent strength-ductility matching was achieved, with a yield strength and tensile strength of 91 J/mm 3 reaching 1061.9 MPa and 1112.2 MPa, respectively, and a fracture strain of 13.21%; the yield strength and tensile strength of 164 J/mm 3 reach 1028.8 MPa and 1063.7 MPa, respectively, with a fracture strain of 10.97%.

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Publication Details

Journal
Journal of Materials Research and Technology
Published
2025-03-01
DOI
https://doi.org/10.1016/j.jmrt.2025.03.033
Citations
4
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
2.85

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article

Grain structure control of a novel titanium alloy during laser powder bed fusion by processing

Minghao Huang, Chao Ding, Shenghang Xu, Shufeng Li et al.
4 citations
Journal of Materials Research and Technology
Additive Manufacturing Materials and Processes
2.85
article

Grain structure control of a novel titanium alloy during laser powder bed fusion by processing

Minghao Huang, Chao Ding, Shenghang Xu, Shufeng Li, Chunnan Song, Huiping Tang, Liying Wu, Xin Yang, Zhaoyang Zhang, Huan Qi
article en
4 citations

Abstract

The characteristic of rapid solidification in additive manufacturing can address the challenge of brittle fracture caused by the segregation of O and Fe atoms in titanium alloys. This paper studied the effects of process parameters of L-PBF and heat treatment on the microstructure and mechanical properties of Ti-0.4O-3Fe alloy. The research indicated that equiaxed prior-β grains were obtained at a low energy density (91J/mm 3 ), while columnar prior-β grains were obtained at a high energy density (164J/mm 3 ). Meanwhile, the α' martensite of less than 1 μm in size and GB-α were distributed in the intracrystalline and grain boundaries of the prior-β grains, respectively. The as-fabricated state of the L-PBF process exhibited high strength but compromised ductility. After annealing at 600°C for 2 hours, excellent strength-ductility matching was achieved, with a yield strength and tensile strength of 91 J/mm 3 reaching 1061.9 MPa and 1112.2 MPa, respectively, and a fracture strain of 13.21%; the yield strength and tensile strength of 164 J/mm 3 reach 1028.8 MPa and 1063.7 MPa, respectively, with a fracture strain of 10.97%.

Journal of Materials Research and TechnologyVol. 35
Xi’an University (CN), Xi'an University of Technology (CN), Hangzhou City University
National Natural Science Foundation of China, National Key Research and Development Program of China
Openalex Percentile: Top 11%
Additive Manufacturing Materials and Processes
2.85
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Grain structure control of a novel titanium alloy during laser powder bed fusion by processing — Minghao Huang, Chao Ding, et al. · Journal of Materials Research and Technology (2025) | TGRS Research Map | TGRS