Microstructure and very high cycle fatigue characteristics of powder bed fused – laser beam (PBF-LB) scandium-free Al-Mg-Zr alloy

This study investigates the microstructure and very high cycle fatigue (VHCF) behavior of a powder bed fusion–laser beam (PBF-LB) processed scandium-free Al-Mg-Zr alloy (commercially known as EOS Al5X1) through advanced microstructural characterization, defect analysis, ultrasonic fatigue testing, and detailed fractographic examination. The analysis focuses on defect-driven crack initiation, particularly process-induced volumetric defects such as pores, lack of fusion, and non-metallic (oxide) inclusions. Scanning electron microscopy-based fractography reveals that in the VHCF regime, where the number of cycles to failure (N f ) > 10 7 cycles, fatigue crack initiation predominantly shifts toward the subsurface or interior of the specimen. In multiple cases, process-induced volumetric defects facilitated crack initiation, resulting in characteristic 'fisheye' fracture morphologies. The chemical composition of these critical defects was also analyzed in detail. The study highlights the significant impact of process-induced volumetric defects on fracture morphology and examines the influence of defect size and location on VHCF performance. These findings provide deeper insight into the interplay between processing defects and crack nucleation, underscoring the necessity of advanced defect characterization to better understand VHCF life variability.

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Publication Details

Journal
Materials Science and Engineering A
Published
2025-03-07
DOI
https://doi.org/10.1016/j.msea.2025.148177
Citations
6
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
4.28
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article

Microstructure and very high cycle fatigue characteristics of powder bed fused – laser beam (PBF-LB) scandium-free Al-Mg-Zr alloy

Marta Gajewska, Shawkat Imam Shakil, Meysam Haghshenas, Zaynab Mahbooba et al.
6 citations
Materials Science and Engineering A
Additive Manufacturing Materials and Processes
4.28
article

Microstructure and very high cycle fatigue characteristics of powder bed fused – laser beam (PBF-LB) scandium-free Al-Mg-Zr alloy

Marta Gajewska, Shawkat Imam Shakil, Meysam Haghshenas, Zaynab Mahbooba, Davide Salvatore Paolino, Andrea Tridello, Wiktor Bednarczyk, Ankit Saharan
article en
6 citations

Abstract

This study investigates the microstructure and very high cycle fatigue (VHCF) behavior of a powder bed fusion–laser beam (PBF-LB) processed scandium-free Al-Mg-Zr alloy (commercially known as EOS Al5X1) through advanced microstructural characterization, defect analysis, ultrasonic fatigue testing, and detailed fractographic examination. The analysis focuses on defect-driven crack initiation, particularly process-induced volumetric defects such as pores, lack of fusion, and non-metallic (oxide) inclusions. Scanning electron microscopy-based fractography reveals that in the VHCF regime, where the number of cycles to failure (N f ) > 10 7 cycles, fatigue crack initiation predominantly shifts toward the subsurface or interior of the specimen. In multiple cases, process-induced volumetric defects facilitated crack initiation, resulting in characteristic 'fisheye' fracture morphologies. The chemical composition of these critical defects was also analyzed in detail. The study highlights the significant impact of process-induced volumetric defects on fracture morphology and examines the influence of defect size and location on VHCF performance. These findings provide deeper insight into the interplay between processing defects and crack nucleation, underscoring the necessity of advanced defect characterization to better understand VHCF life variability.

Materials Science and Engineering AVol. 930
Jagiellonian University (PL), Politecnico di Torino (IT), Pflugerville Independent School District (US), AGH University of Krakow (PL), University of Toledo (US)
Openalex Percentile: Top 6%
Additive Manufacturing Materials and Processes
4.28
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