Evaluation of polymer viscoelasticity by integrated micro-indentation test with optical flow algorithm

This study aims to directly evaluate the viscoelastic (creep) parameters of polymer materials by integrating a micro-indentation test with an optical flow (OF) algorithm and an embedded center of dilatation (ECD) model. After indentation, the in-plane displacement field on the specimen surface is measured over time using the OF algorithm, thereby capturing the recovery behavior of the indentation imprint. Subsequently, the creep strain evolution curve over time is obtained through displacement and spatial differentiation. The ECD model is employed to estimate the initial residual stress induced by indentation process without resorting to complex inverse analysis. The reliability of estimated surface residual stress was validated through FEA. A time hardening model is then used to derive the creep strain-time relationship. Using the initial residual stress and the creep strain curve obtained from indentation, the time hardening creep parameters are determined. The experimental tests on polymethyl methacrylate (PMMA) and polycarbonate (PC) have demonstrated that the proposed method yields creep parameters within an approximate 5% error margin relative to conventional tensile creep tests. • An integrated approach using indentation tests and optical flow evaluates polymer viscoelasticity. • The surface residual stress induced by indentation is estimated via embedded center of dilatation model. • Creep model parameters derived from the recovery of in-plane indentation displacement fields. • The accuracy of the proposed method is validated through a comparison with conventional uniaxial creep tests.

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Publication Details

Journal
Polymer Testing
Published
2025-02-28
DOI
https://doi.org/10.1016/j.polymertesting.2025.108750
Citations
3
Primary Topic
Advanced Surface Polishing Techniques
Type
article
Field-Weighted Citation Impact
2.02

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article

Evaluation of polymer viscoelasticity by integrated micro-indentation test with optical flow algorithm

Hyungyil Lee, Giyeol Han, Yeo-Choon Yoon
3 citations
Polymer Testing
Advanced Surface Polishing Techniques
2.02
article

Evaluation of polymer viscoelasticity by integrated micro-indentation test with optical flow algorithm

Hyungyil Lee, Giyeol Han, Yeo-Choon Yoon
article en
3 citations

Abstract

This study aims to directly evaluate the viscoelastic (creep) parameters of polymer materials by integrating a micro-indentation test with an optical flow (OF) algorithm and an embedded center of dilatation (ECD) model. After indentation, the in-plane displacement field on the specimen surface is measured over time using the OF algorithm, thereby capturing the recovery behavior of the indentation imprint. Subsequently, the creep strain evolution curve over time is obtained through displacement and spatial differentiation. The ECD model is employed to estimate the initial residual stress induced by indentation process without resorting to complex inverse analysis. The reliability of estimated surface residual stress was validated through FEA. A time hardening model is then used to derive the creep strain-time relationship. Using the initial residual stress and the creep strain curve obtained from indentation, the time hardening creep parameters are determined. The experimental tests on polymethyl methacrylate (PMMA) and polycarbonate (PC) have demonstrated that the proposed method yields creep parameters within an approximate 5% error margin relative to conventional tensile creep tests. • An integrated approach using indentation tests and optical flow evaluates polymer viscoelasticity. • The surface residual stress induced by indentation is estimated via embedded center of dilatation model. • Creep model parameters derived from the recovery of in-plane indentation displacement fields. • The accuracy of the proposed method is validated through a comparison with conventional uniaxial creep tests.

Polymer TestingVol. 145
Sogang University (KR), Japan Display (Japan) (JP)
National Research Foundation of Korea
Openalex Percentile: Top 15%
Advanced Surface Polishing Techniques
2.02
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