Microstructure and Texture Evolution of High Permeability Grain-Oriented Silicon Steel

Industrialization trial production of high permeability (Hi-B) steel was carried out by “one cold rolled + decarburization and nitridation technologies”. The finished product reached the level of 23Q100 with an average grain size of 5.47 cm, magnetic flux density B8 of 1.902T, and the iron loss P1.7/50 of 0.975 W/Kg. The evolution law of the microstructure and texture under different processes was analyzed with the help of OM, EBSD, and XRD. The results showed that the microstructure of the hot rolled plate was equiaxed crystals in the surface layer, a mixture of recrystallization grains and banded fiber in the quarter of the thickness layer, and banded fiber in the center layer. The texture gradient of the hot rolled plate from the surface layer to the center layer was {112}<111> + {110}<114> → {441}<014> → {001}~{111}<110>. The texture of the normalized plate was in major {110}<113> in the surface layer, diffuse α-fiber texture and {441}<014> in the quarter of the thickness layer, and sharp α texture {001}~{111}<110> in the center layer. The texture of the cold-rolled sheet was concentrated in {001}~{332}<110>. The average grain size of the decarburizing and nitriding sheet was 26.4 μm, and the texture of the first recrystallization is sharp α*-fiber and weak {111}<112>. The finished product has a sharp single Goss texture. For Hi-B steel, the Goss secondary nucleus originated from the surface layer to 1/4 layer of the hot rolled plate and reached the highest content of 11.5% in the quarter of the thickness. The content of the Goss texture decreased with the subsequent normalization and cold rolling, then the Goss grains nucleated again during the decarburization annealing and high temperature annealing processes.