Powder bed fusion on single lines of Cu-doped hydroxyapatite powder bed

• Laser-hydroxyapatite material interaction was used to produce ceramics delaminated ribbons (CDR) or anchored ribbons (CAR). • CDRs exhibit surface/bulk density gradients due to thermal conductivity / Mie scattering limiting laser penetration. • Crack patterning observed on CARs is correlated to the material’s isotherms during laser sintering. • CARs show “sandwich morphology” with a porous intermediate layer in between top and bottom dense layers due to substrate/film interface effect. This study aims to design ceramic scaffolds for precise bone reconstruction using Powder Bed Laser Sintering (PBLS) to create cohesive Cu-doped HAp ribbons from a single lasered line on a thin powder bed atop a silicate lime substrate. Depending on laser parameters, two ribbon types—delaminated (CDR) or anchored (CAR)—are produced, both exhibiting surface density gradients from the center to the edges. Microscale analysis reveals surface density gradients in both ribbon types, extending from center to edge. CDRs also show depth-wise density variations, resulting in mechanical stresses that cause detachment and curling. In CARs, intense local heating and thermal conductivity cause a temperature rise beyond the irradiated area. The substrate acts as a thermal barrier, concentrating heat at the film-substrate interface and ensuring ribbon adhesion. Cracks propagate perpendicular to isothermal lines, enabling controlled crack patterning.

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Publication Details

Journal
Materials & Design
Published
2025-02-22
DOI
https://doi.org/10.1016/j.matdes.2025.113757
Citations
1
Primary Topic
Additive Manufacturing and 3D Printing Technologies
Type
article
Field-Weighted Citation Impact
0.68
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article

Powder bed fusion on single lines of Cu-doped hydroxyapatite powder bed

François Rouzé l’Alzit, Manuel Gaudon, Thierry Cardinal, Benoît Glorieux
1 citations
Materials & Design
Additive Manufacturing and 3D Printing Technologies
0.68
article

Powder bed fusion on single lines of Cu-doped hydroxyapatite powder bed

François Rouzé l’Alzit, Manuel Gaudon, Thierry Cardinal, Benoît Glorieux
article en
1 citations

Abstract

• Laser-hydroxyapatite material interaction was used to produce ceramics delaminated ribbons (CDR) or anchored ribbons (CAR). • CDRs exhibit surface/bulk density gradients due to thermal conductivity / Mie scattering limiting laser penetration. • Crack patterning observed on CARs is correlated to the material’s isotherms during laser sintering. • CARs show “sandwich morphology” with a porous intermediate layer in between top and bottom dense layers due to substrate/film interface effect. This study aims to design ceramic scaffolds for precise bone reconstruction using Powder Bed Laser Sintering (PBLS) to create cohesive Cu-doped HAp ribbons from a single lasered line on a thin powder bed atop a silicate lime substrate. Depending on laser parameters, two ribbon types—delaminated (CDR) or anchored (CAR)—are produced, both exhibiting surface density gradients from the center to the edges. Microscale analysis reveals surface density gradients in both ribbon types, extending from center to edge. CDRs also show depth-wise density variations, resulting in mechanical stresses that cause detachment and curling. In CARs, intense local heating and thermal conductivity cause a temperature rise beyond the irradiated area. The substrate acts as a thermal barrier, concentrating heat at the film-substrate interface and ensuring ribbon adhesion. Cracks propagate perpendicular to isothermal lines, enabling controlled crack patterning.

Materials & DesignVol. 252
Centre National de la Recherche Scientifique (FR), Institut de Chimie de la Matière Condensée de Bordeaux (FR)
Openalex Percentile: Top 34%
Additive Manufacturing and 3D Printing Technologies
0.68
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Powder bed fusion on single lines of Cu-doped hydroxyapatite powder bed — François Rouzé l’Alzit, Manuel Gaudon, et al. · Materials & Design (2025) | TGRS Research Map | TGRS