Study of structural, mechanical and thermal properties of chitosan/PVA blend by casting method in different proportions

Chitosan and a combination of Chitosan and PVA with varying PVA weight ratios (5, 10, 15, 20, and 25%) are created using the solution casting technique. The produced samples underwent structural, mechanical, and thermal tests using X-ray diffraction (XRD), Fourier-transformed infrared spectroscopy (FTIR), strain stress test, hardness test, thermal conductivity test, and antibacterial test. The XRD measurements confirm the purity of the Chitosan and PVA powders. Furthermore, the observed alteration in the energy levels of some FTIR bands for polysaccharides, along with a decrease in their intensities, suggests the occurrence of Chitosan: PVA blend synthesis. The highest values for tensile strength, hardness, and thermal conductivity are observed at a PVA ratio of 10%. The antibacterial activity of the chitosan/PVA blends is assessed using the inhibitory concentration technique. The results indicate varying levels of activity among the different samples. The Chitosan/PVA combination at a 15% blend ratio exhibited the greatest suppression of the microorganisms. The mix exhibits lower efficacy against gram-positive bacteria compared to gram-negative bacteria.

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Publication Details

Journal
Experimental and Theoretical NANOTECHNOLOGY
Published
2025-02-15
DOI
https://doi.org/10.56053/9.s.167
Primary Topic
Nanocomposite Films for Food Packaging
Type
article
Field-Weighted Citation Impact
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article

Study of structural, mechanical and thermal properties of chitosan/PVA blend by casting method in different proportions

Ahmed Jadah Farhan, Fazli Hadi
Experimental and Theoretical NANOTECHNOLOGY
Nanocomposite Films for Food Packaging
article

Study of structural, mechanical and thermal properties of chitosan/PVA blend by casting method in different proportions

Ahmed Jadah Farhan, Fazli Hadi
article en

Abstract

Chitosan and a combination of Chitosan and PVA with varying PVA weight ratios (5, 10, 15, 20, and 25%) are created using the solution casting technique. The produced samples underwent structural, mechanical, and thermal tests using X-ray diffraction (XRD), Fourier-transformed infrared spectroscopy (FTIR), strain stress test, hardness test, thermal conductivity test, and antibacterial test. The XRD measurements confirm the purity of the Chitosan and PVA powders. Furthermore, the observed alteration in the energy levels of some FTIR bands for polysaccharides, along with a decrease in their intensities, suggests the occurrence of Chitosan: PVA blend synthesis. The highest values for tensile strength, hardness, and thermal conductivity are observed at a PVA ratio of 10%. The antibacterial activity of the chitosan/PVA blends is assessed using the inhibitory concentration technique. The results indicate varying levels of activity among the different samples. The Chitosan/PVA combination at a 15% blend ratio exhibited the greatest suppression of the microorganisms. The mix exhibits lower efficacy against gram-positive bacteria compared to gram-negative bacteria.

Experimental and Theoretical NANOTECHNOLOGYVol. 9(S)
University of Wasit (IQ)
Openalex Percentile: Top 98%
Nanocomposite Films for Food Packaging
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