The Effect of Chemical Surface Modification on the Repair Bond Strength of Resin Composite: An In Vitro Study

This in vitro study investigates the impact of the chemical modification of resin composite surfaces on repair bond strength of micro-hybrid resin composite material. First, 7 mm circular × 3 mm thick resin composite disks were prepared using teflon molds. Then, 50 specimens out of 100 were allocated for stimulated aging using a thermo-cycling (10,000 cycles) device. Both the 24 h and 1-year-aged composite discs were embedded in epoxy resin using a 2.5 cm wide × 1.5 cm thick circular mold. The surfaces were treated with Clearfil S3 bond alone or with the additional application of silane or porcelain primer. The other two groups were bonded with CRB bond with or without a porcelain primer. Using a teflon mold, a 2 mm circular and 3 mm high repair composite cylinder was built on the treated surfaces. The specimens were then stressed to de-bond by applying shear force to measure repair bond strength, and they were observed under the microscope to determine the failure pattern. The data were analyzed using SPSS26.0. Univariate analysis showed a significant effect (<i>p</i> = 0.013) of the bonding protocol on the repair bond strength; however, the effect of aging was insignificant (<i>p</i> = 0.170). The S3 bond with additional silane and the CRB bond showed the significantly higher repair bond strength of the 1-year-aged micro-hybrid composite. However, in case of 24 h aged specimens, the repair bond strength was statistically insignificant among the tested groups (<i>p</i> = 0.340). Chemical surface modification with silane has the potential to improve the repair bond strength of micro-hybrid resin composite materials.

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Publication Details

Journal
Polymers
Published
2025-02-16
DOI
https://doi.org/10.3390/polym17040513
Citations
4
Primary Topic
Dental materials and restorations
Type
article
Field-Weighted Citation Impact
6.70
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article

The Effect of Chemical Surface Modification on the Repair Bond Strength of Resin Composite: An In Vitro Study

Shadi El Bahra, Md Sofiqul Islam, Smriti Aryal A C, A. Tawil et al.
4 citations
Polymers
Dental materials and restorations
6.70
article

The Effect of Chemical Surface Modification on the Repair Bond Strength of Resin Composite: An In Vitro Study

Shadi El Bahra, Md Sofiqul Islam, Smriti Aryal A C, A. Tawil, Ihab Sabri Saleh, Vivek Padmanabhan, Upoma Guha, Muhammed Mustahsen Rahman
article en
4 citations

Abstract

This in vitro study investigates the impact of the chemical modification of resin composite surfaces on repair bond strength of micro-hybrid resin composite material. First, 7 mm circular × 3 mm thick resin composite disks were prepared using teflon molds. Then, 50 specimens out of 100 were allocated for stimulated aging using a thermo-cycling (10,000 cycles) device. Both the 24 h and 1-year-aged composite discs were embedded in epoxy resin using a 2.5 cm wide × 1.5 cm thick circular mold. The surfaces were treated with Clearfil S3 bond alone or with the additional application of silane or porcelain primer. The other two groups were bonded with CRB bond with or without a porcelain primer. Using a teflon mold, a 2 mm circular and 3 mm high repair composite cylinder was built on the treated surfaces. The specimens were then stressed to de-bond by applying shear force to measure repair bond strength, and they were observed under the microscope to determine the failure pattern. The data were analyzed using SPSS26.0. Univariate analysis showed a significant effect (<i>p</i> = 0.013) of the bonding protocol on the repair bond strength; however, the effect of aging was insignificant (<i>p</i> = 0.170). The S3 bond with additional silane and the CRB bond showed the significantly higher repair bond strength of the 1-year-aged micro-hybrid composite. However, in case of 24 h aged specimens, the repair bond strength was statistically insignificant among the tested groups (<i>p</i> = 0.340). Chemical surface modification with silane has the potential to improve the repair bond strength of micro-hybrid resin composite materials.

PolymersVol. 17(4)
University of Sharjah (AE), University of Nebraska Medical Center (US), Ras al-Khaimah Medical and Health Sciences University (AE)
Openalex Percentile: Top 4%
Dental materials and restorations
6.70
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