Microencapsulation of L-carvone and hexyl salicylate in carnauba wax, candelilla wax and beeswax by melt dispersion method

Wax microspheres encapsulating flavour or fragrance oil (L-carvone, Hexyl salicylate) prepared via melt dispersion was investigated. This study highlights the influence of different waxes as well as variable oil loadings on the fundamental properties of the resulting microparticles. The mechanical characterisation of individual wax microspheres by a micromanipulation technique is firstly reported here and the values of Young's modulus of wax microspheres were determined by fitting the experimental force versus displacement with the Hertz model. The relation between the payload and Young's modulus of wax microsphere was also explored in this study. • Encapsulation of 2 model oils (hexyl salicylate and L-carvone) using sustainable waxes. • Characterisation of the mechanical properties of wax microcapsules using a micromanipulation technique. • Candelilla wax demonstrating the highest encapsulation efficiency at 72 % for hexyl salicylate. • The oil payload of wax microspheres increasing with the oil-to-wax ratio. • Young's modulusdecreasing significantly with increasing the oil-to-wax ratio.

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Publication Details

Journal
Polymer Testing
Published
2025-02-01
DOI
https://doi.org/10.1016/j.polymertesting.2025.108728
Citations
3
Primary Topic
Microencapsulation and Drying Processes
Type
article
Field-Weighted Citation Impact
3.49
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article

Microencapsulation of L-carvone and hexyl salicylate in carnauba wax, candelilla wax and beeswax by melt dispersion method

Zhibing Zhang
3 citations
Polymer Testing
Microencapsulation and Drying Processes
3.49
article

Microencapsulation of L-carvone and hexyl salicylate in carnauba wax, candelilla wax and beeswax by melt dispersion method

Zhibing Zhang
article en
3 citations

Abstract

Wax microspheres encapsulating flavour or fragrance oil (L-carvone, Hexyl salicylate) prepared via melt dispersion was investigated. This study highlights the influence of different waxes as well as variable oil loadings on the fundamental properties of the resulting microparticles. The mechanical characterisation of individual wax microspheres by a micromanipulation technique is firstly reported here and the values of Young's modulus of wax microspheres were determined by fitting the experimental force versus displacement with the Hertz model. The relation between the payload and Young's modulus of wax microsphere was also explored in this study. • Encapsulation of 2 model oils (hexyl salicylate and L-carvone) using sustainable waxes. • Characterisation of the mechanical properties of wax microcapsules using a micromanipulation technique. • Candelilla wax demonstrating the highest encapsulation efficiency at 72 % for hexyl salicylate. • The oil payload of wax microspheres increasing with the oil-to-wax ratio. • Young's modulusdecreasing significantly with increasing the oil-to-wax ratio.

Polymer TestingVol. 143
University of Birmingham (GB)
Zero hunger
Openalex Percentile: Top 10%
Microencapsulation and Drying Processes
3.49
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