Radiation Damage Mitigation in FeCrAl Alloy at Sub-Recrystallization Temperatures

Traditional defect recovery methods rely on high-temperature annealing, often exceeding 750 °C for FeCrAl. In this study, we introduce electron wind force (EWF)-assisted annealing as an alternative approach to mitigate irradiation-induced defects at significantly lower temperatures. FeCrAl samples irradiated with 5 MeV Zr<sup>2+</sup> ions at a dose of 10<sup>14</sup> cm<sup>-2</sup> were annealed using EWF at 250 °C for 60 s. We demonstrate a remarkable transformation in the irradiated microstructure, where significant increases in kernel average misorientation (KAM) and low-angle grain boundaries (LAGBs) typically indicate heightened defect density; the use of EWF annealing reversed these effects. X-ray diffraction (XRD) confirmed these findings, showing substantial reductions in full width at half maximum (FWHM) values and a realignment of peak positions toward their original states, indicative of stress and defect recovery. To compare the effectiveness of EWF, we also conducted traditional thermal annealing at 250 °C for 7 h, which proved less effective in defect recovery as evidenced by less pronounced improvements in XRD FWHM values.

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Publication Details

Journal
Materials
Published
2024-12-31
DOI
https://doi.org/10.3390/ma18010124
Citations
4
Primary Topic
Nuclear Materials and Properties
Type
article
Field-Weighted Citation Impact
0.47

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article

Radiation Damage Mitigation in FeCrAl Alloy at Sub-Recrystallization Temperatures

Daudi Waryoba, Md Abu Jafar Rasel, Aman Haque, Christopher M. Smyth et al.
4 citations
Materials
Nuclear Materials and Properties
0.47
article

Radiation Damage Mitigation in FeCrAl Alloy at Sub-Recrystallization Temperatures

Daudi Waryoba, Md Abu Jafar Rasel, Aman Haque, Christopher M. Smyth, Md Hafijur Rahman
article en
4 citations

Abstract

Traditional defect recovery methods rely on high-temperature annealing, often exceeding 750 °C for FeCrAl. In this study, we introduce electron wind force (EWF)-assisted annealing as an alternative approach to mitigate irradiation-induced defects at significantly lower temperatures. FeCrAl samples irradiated with 5 MeV Zr<sup>2+</sup> ions at a dose of 10<sup>14</sup> cm<sup>-2</sup> were annealed using EWF at 250 °C for 60 s. We demonstrate a remarkable transformation in the irradiated microstructure, where significant increases in kernel average misorientation (KAM) and low-angle grain boundaries (LAGBs) typically indicate heightened defect density; the use of EWF annealing reversed these effects. X-ray diffraction (XRD) confirmed these findings, showing substantial reductions in full width at half maximum (FWHM) values and a realignment of peak positions toward their original states, indicative of stress and defect recovery. To compare the effectiveness of EWF, we also conducted traditional thermal annealing at 250 °C for 7 h, which proved less effective in defect recovery as evidenced by less pronounced improvements in XRD FWHM values.

MaterialsVol. 18(1)
Pennsylvania State University (US), Sandia National Laboratories (US)
Army Research Office
Affordable and clean energy
Openalex Percentile: Top 37%
Nuclear Materials and Properties
0.47
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