Radiation Damage Mitigation in FeCrAl Alloy at Sub-Recrystallization Temperatures
Traditional defect recovery methods rely on high-temperature annealing, often exceeding 750 °C for FeCrAl. In this study, we introduce electron wind force (EWF)-assisted annealing as an alternative approach to mitigate irradiation-induced defects at significantly lower temperatures. FeCrAl samples irradiated with 5 MeV Zr<sup>2+</sup> ions at a dose of 10<sup>14</sup> cm<sup>-2</sup> were annealed using EWF at 250 °C for 60 s. We demonstrate a remarkable transformation in the irradiated microstructure, where significant increases in kernel average misorientation (KAM) and low-angle grain boundaries (LAGBs) typically indicate heightened defect density; the use of EWF annealing reversed these effects. X-ray diffraction (XRD) confirmed these findings, showing substantial reductions in full width at half maximum (FWHM) values and a realignment of peak positions toward their original states, indicative of stress and defect recovery. To compare the effectiveness of EWF, we also conducted traditional thermal annealing at 250 °C for 7 h, which proved less effective in defect recovery as evidenced by less pronounced improvements in XRD FWHM values.
Authors
- Daudi Waryoba (ORCID: https://orcid.org/0000-0002-1190-3665)
- Md Abu Jafar Rasel (ORCID: https://orcid.org/0009-0003-1866-6767)
- Aman Haque (ORCID: https://orcid.org/0000-0001-6535-5484)
- Christopher M. Smyth (ORCID: https://orcid.org/0000-0003-4668-9555)
- Md Hafijur Rahman (ORCID: https://orcid.org/0000-0002-1440-1839)
Institutions
- Pennsylvania State University (US)
- Sandia National Laboratories (US)
Publication Details
- Journal
- Materials
- Published
- 2024-12-31
- DOI
- https://doi.org/10.3390/ma18010124
- Citations
- 4
- Primary Topic
- Nuclear Materials and Properties
- Type
- article
- Field-Weighted Citation Impact
- 0.47
Funders
- Army Research Office