Synthesis and Characterization of Poly (Ester‐Imide) S Based on Imide Dicarboxylic Acid with Dihydroxy Heterocyclic Compounds

By using dibutyltine dilaurate as a catalyst in the polycondensation of imide dicarboxylic acid and aromatic diols, two thermally stable and organosoluble poly(ester-imide) s were created. One mole of orthochlorobenzaldehyde and 2,4-dichlorobenzaldehyde was condensed, respectively, with p-hydroxy acetophenone to yield two phenolic compounds. Two Imide compounds were prepared from the reaction of Pyromellitic anhydride, and 3,3,4-benzophenone tetracarboxylic dianhydride with anthranilic acid respectively. The structural properties of the poly (esters-imide)'s were verified by FTIR, 1H NMR, and 13C NMR spectroscopy analysis of the synthesized polymers.

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Publication Details

Journal
Medical Science Journal for Advance Research
Published
2024-12-31
DOI
https://doi.org/10.46966/msjar.v5i4.235
Primary Topic
Synthesis and properties of polymers
Type
article
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article

Synthesis and Characterization of Poly (Ester‐Imide) S Based on Imide Dicarboxylic Acid with Dihydroxy Heterocyclic Compounds

Nadia Baqer Hussein
3 links
Medical Science Journal for Advance Research
Synthesis and properties of polymers
article

Synthesis and Characterization of Poly (Ester‐Imide) S Based on Imide Dicarboxylic Acid with Dihydroxy Heterocyclic Compounds

Nadia Baqer Hussein
article en

Abstract

By using dibutyltine dilaurate as a catalyst in the polycondensation of imide dicarboxylic acid and aromatic diols, two thermally stable and organosoluble poly(ester-imide) s were created. One mole of orthochlorobenzaldehyde and 2,4-dichlorobenzaldehyde was condensed, respectively, with p-hydroxy acetophenone to yield two phenolic compounds. Two Imide compounds were prepared from the reaction of Pyromellitic anhydride, and 3,3,4-benzophenone tetracarboxylic dianhydride with anthranilic acid respectively. The structural properties of the poly (esters-imide)'s were verified by FTIR, 1H NMR, and 13C NMR spectroscopy analysis of the synthesized polymers.

Medical Science Journal for Advance ResearchVol. 5(4)
University of Al-Qadisiyah (IQ)
Clean water and sanitation
Openalex Percentile: Top 80%
Synthesis and properties of polymers
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