Application of Square-Wave Stripping Voltammetry for the Analysis of Electrodeposits Based on Lead-Bismuth

The possibility of targeted electrodeposition of coatings in the lead-bismuth binary system is discussed. The analysis of metal content in electrodeposits was performed using square-wave stripping voltammetry of solutions simultaneously containing lead and bismuth. The obtained results were supported by scanning electron microscopy, energy-dispersive X-ray spectroscopy, and powder X-ray diffraction analysis. The electrodeposition conditions of obtaining Pb7Bi3 ε-phase, which is promising for the application in superconducting microelectronics, were found.

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Journal
Электрохимия
Published
2024-08-15
DOI
https://doi.org/10.31857/s0424857024080013
Primary Topic
Electrochemical Analysis and Applications
Type
article
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article

Application of Square-Wave Stripping Voltammetry for the Analysis of Electrodeposits Based on Lead-Bismuth

Kirill Napolsky, I. V. Kolesnik, Stepan V. Sotnichuk, I Voronin
Электрохимия
Electrochemical Analysis and Applications
article

Application of Square-Wave Stripping Voltammetry for the Analysis of Electrodeposits Based on Lead-Bismuth

Kirill Napolsky, I. V. Kolesnik, Stepan V. Sotnichuk, I Voronin
article en

Abstract

The possibility of targeted electrodeposition of coatings in the lead-bismuth binary system is discussed. The analysis of metal content in electrodeposits was performed using square-wave stripping voltammetry of solutions simultaneously containing lead and bismuth. The obtained results were supported by scanning electron microscopy, energy-dispersive X-ray spectroscopy, and powder X-ray diffraction analysis. The electrodeposition conditions of obtaining Pb7Bi3 ε-phase, which is promising for the application in superconducting microelectronics, were found.

ЭлектрохимияVol. 60(8)
Lomonosov Moscow State University (RU), NS Kurnakova Institute of General and Inorganic Chemistry (RU), Moscow State University (TJ)
Openalex Percentile: Top 76%
Electrochemical Analysis and Applications
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Application of Square-Wave Stripping Voltammetry for the Analysis of Electrodeposits Based on Lead-Bismuth — Kirill Napolsky, I. V. Kolesnik, et al. · Электрохимия (2024) | TGRS Research Map | TGRS