Amine Oxide: Synthesis and Analysis

This paper presents the laboratory synthesis of zwitterionic surfactant—oleylamido propyldimethylamine oxide (OADAO), as well as the selection of conditions for its implementation. The results of the analysis of synthesis products by potentiometric titration and IR-Fourier spectroscopy methods are presented, which prove the presence of the target product in the composition of the reaction mass at the end of synthesis. The positive results of the synthesis and the absence of light organochlorine compounds (LOC) in the end products allow us to further consider OADAO, for example, as a gelling agent for aqueous fracturing fluids, by studying its technological characteristics.

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Published
2024-11-14
DOI
https://doi.org/10.3390/ecsoc-28-20114
Primary Topic
Analytical Chemistry and Chromatography
Type
article
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article

Amine Oxide: Synthesis and Analysis

Mikhail Aleksandrovich Silin, Polina Konstantinovna Krisanova, S.A. Borodin, Л. А. Магадова et al.
Analytical Chemistry and Chromatography
article

Amine Oxide: Synthesis and Analysis

Mikhail Aleksandrovich Silin, Polina Konstantinovna Krisanova, S.A. Borodin, Л. А. Магадова, Andrey Filatov, Mikhail Mikhailovich Muhin, Savely Alekseevich Mityurev
article en

Abstract

This paper presents the laboratory synthesis of zwitterionic surfactant—oleylamido propyldimethylamine oxide (OADAO), as well as the selection of conditions for its implementation. The results of the analysis of synthesis products by potentiometric titration and IR-Fourier spectroscopy methods are presented, which prove the presence of the target product in the composition of the reaction mass at the end of synthesis. The positive results of the synthesis and the absence of light organochlorine compounds (LOC) in the end products allow us to further consider OADAO, for example, as a gelling agent for aqueous fracturing fluids, by studying its technological characteristics.

Gubkin Russian State University of Oil and Gas (RU)
Openalex Percentile: Top 81%
Analytical Chemistry and Chromatography
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