Role of heat treatment in enhancing microstructure and properties of Inconel 625 manufactured by directed energy deposition using wire arc

Inconel 625, a nickel-based superalloy, is known for its exceptional mechanical properties and corrosion resistance, widely utilized in aerospace, marine, and chemical industries. Inconel 625 components fabricated by Directed Energy Deposition using Wire Arc (DED-Wire Arc), exhibit coarse dendritic microstructures and Laves phases in the as-built state, necessitating heat treatments for property enhancement. Heat treatments at 1050–1100 °C improved tensile strength by up to 15–17 % (e.g., from 850 MPa to 980 MPa for DED-Arc) and hardness by 40–52 % (e.g., from 250 HV to 380 HV). Solubilisation effectively dissolved Laves and MC-type carbides, reducing phase fractions to 15 % and promoting a more uniform microstructure. Annealing at 700–900 °C induced γ′ and γ′′ precipitates, optimizing hardness while maintaining elongation. Comparatively, DED-LB and PBF-LB techniques, with finer as-built microstructures, achieved better responses to heat treatments, reaching tensile strengths of 1050 MPa and elongations of 25 % post-solubilisation. Rapid quenching methods controlled recrystallization, reducing grain boundaries and improving corrosion resistance by 32 % in corrosion potential and decreasing passivation current density by 52 %. This study highlights the significant role of heat treatments in enhancing the microstructure and properties of Inconel 625 produced by DED-Wire Arc, positioning it as a reliable candidate for demanding industrial applications. • The study explores how various heat treatments like stress relief, solubilisation, and annealing improve mechanical properties and refine microstructures. • Demonstrates that tensile strength increases by up to 17 % and hardness improves by up to 52 % with optimized heat treatments. • Highlights the microstructural evolution, reducing detrimental Laves phases and forming strengthening precipitates for better performance. • Shows that enhanced corrosion resistance is achieved through effective heat treatments, making the material stable under extreme conditions.

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Publication Details

Journal
Journal of Alloys and Metallurgical Systems
Published
2024-12-26
DOI
https://doi.org/10.1016/j.jalmes.2024.100147
Citations
4
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
0.85
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article

Role of heat treatment in enhancing microstructure and properties of Inconel 625 manufactured by directed energy deposition using wire arc

Ashwin Sailesh, Vipin Sharma, T.S. Senthil, Rahul Singh et al.
4 citations
Journal of Alloys and Metallurgical Systems
Additive Manufacturing Materials and Processes
0.85
article

Role of heat treatment in enhancing microstructure and properties of Inconel 625 manufactured by directed energy deposition using wire arc

Ashwin Sailesh, Vipin Sharma, T.S. Senthil, Rahul Singh, Manickam Ravichandran, K K Arun, Dhivakar Poosapadi, Paranthaman, L Rajasekhara Babu
article en
4 citations

Abstract

Inconel 625, a nickel-based superalloy, is known for its exceptional mechanical properties and corrosion resistance, widely utilized in aerospace, marine, and chemical industries. Inconel 625 components fabricated by Directed Energy Deposition using Wire Arc (DED-Wire Arc), exhibit coarse dendritic microstructures and Laves phases in the as-built state, necessitating heat treatments for property enhancement. Heat treatments at 1050–1100 °C improved tensile strength by up to 15–17 % (e.g., from 850 MPa to 980 MPa for DED-Arc) and hardness by 40–52 % (e.g., from 250 HV to 380 HV). Solubilisation effectively dissolved Laves and MC-type carbides, reducing phase fractions to 15 % and promoting a more uniform microstructure. Annealing at 700–900 °C induced γ′ and γ′′ precipitates, optimizing hardness while maintaining elongation. Comparatively, DED-LB and PBF-LB techniques, with finer as-built microstructures, achieved better responses to heat treatments, reaching tensile strengths of 1050 MPa and elongations of 25 % post-solubilisation. Rapid quenching methods controlled recrystallization, reducing grain boundaries and improving corrosion resistance by 32 % in corrosion potential and decreasing passivation current density by 52 %. This study highlights the significant role of heat treatments in enhancing the microstructure and properties of Inconel 625 produced by DED-Wire Arc, positioning it as a reliable candidate for demanding industrial applications. • The study explores how various heat treatments like stress relief, solubilisation, and annealing improve mechanical properties and refine microstructures. • Demonstrates that tensile strength increases by up to 17 % and hardness improves by up to 52 % with optimized heat treatments. • Highlights the microstructural evolution, reducing detrimental Laves phases and forming strengthening precipitates for better performance. • Shows that enhanced corrosion resistance is achieved through effective heat treatments, making the material stable under extreme conditions.

Journal of Alloys and Metallurgical SystemsVol. 9
Shenyang Ligong University (CN), SRM Institute of Science and Technology (IN), National Institute of Ocean Technology (IN), Sri Ramakrishna Institute of Paramedical Sciences (IN), Medi-Caps University (IN), Orthopaedic Research Group (IN), Global Services (Slovakia) (SK), Koneru Lakshmaiah Education Foundation (IN), Noorul Islam University (IN)
Affordable and clean energy
Openalex Percentile: Top 29%
Additive Manufacturing Materials and Processes
0.85
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