Evaluation of 3D-printed plastics for Ultra-High Vacuum applications: Outgassing, and residual gas analysis

The demand for cost- and time-effective and customizable components for High Vacuum (HV) and Ultra-High Vacuum (UHV) systems has prompted exploration into the application of 3D-printing technology. This study investigates the viability of utilizing 3D-printed plastics in UHV environments by evaluating their outgassing properties. An extensive evaluation of 3D-printing materials was carried out, highlighting the best polymer candidates using two of the most common 3D-printing techniques, Fused Deposition Modelling (Crump, 1992; Upcraft and Fletcher, 2003) [1] , [2] and Stereolithography (Hull, 1986; Upcraft and Fletcher, 2003) [2] , [3] . Further experimental investigations were conducted to assess the performance of select 3D-printed plastics under UHV conditions, focusing on their low outgassing and resistance to baking temperatures. Furthermore, residual gas analysis was used to evaluate the materials compatibility with Non-Evaporable Getter coated systems and possible presence of other contaminants. The findings suggest that certain 3D-printed plastics exhibit promising characteristics for use in HV and UHV systems, with notable examples including cyclic olefin copolymer and polyetheretherketone along with Rigid 10K and Tullomer™. A comparison between machined and 3D-printed parts demonstrated that challenges such as porosity and surface roughness showed not to be a cause of great concern. • Ultra-high vacuum compatible 3D-printed plastics. • 3D-printed versus machined PEEK, vacuum compatibility comparison. • Outgassing properties of FDM and SLA printed materials assessed. • Low outgassing polymers: PEEK, Rigid 10K, COC, and Tullomer™.

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Publication Details

Journal
Vacuum
Published
2024-12-25
DOI
https://doi.org/10.1016/j.vacuum.2024.113970
Citations
3
Primary Topic
Additive Manufacturing and 3D Printing Technologies
Type
article
Field-Weighted Citation Impact
0.61

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article

Evaluation of 3D-printed plastics for Ultra-High Vacuum applications: Outgassing, and residual gas analysis

Artur Domingues Tavares de Sá, Ana Martínez-Carboneres, Stefan Carlson
3 citations
Vacuum
Additive Manufacturing and 3D Printing Technologies
0.61
article

Evaluation of 3D-printed plastics for Ultra-High Vacuum applications: Outgassing, and residual gas analysis

Artur Domingues Tavares de Sá, Ana Martínez-Carboneres, Stefan Carlson
article en
3 citations

Abstract

The demand for cost- and time-effective and customizable components for High Vacuum (HV) and Ultra-High Vacuum (UHV) systems has prompted exploration into the application of 3D-printing technology. This study investigates the viability of utilizing 3D-printed plastics in UHV environments by evaluating their outgassing properties. An extensive evaluation of 3D-printing materials was carried out, highlighting the best polymer candidates using two of the most common 3D-printing techniques, Fused Deposition Modelling (Crump, 1992; Upcraft and Fletcher, 2003) [1] , [2] and Stereolithography (Hull, 1986; Upcraft and Fletcher, 2003) [2] , [3] . Further experimental investigations were conducted to assess the performance of select 3D-printed plastics under UHV conditions, focusing on their low outgassing and resistance to baking temperatures. Furthermore, residual gas analysis was used to evaluate the materials compatibility with Non-Evaporable Getter coated systems and possible presence of other contaminants. The findings suggest that certain 3D-printed plastics exhibit promising characteristics for use in HV and UHV systems, with notable examples including cyclic olefin copolymer and polyetheretherketone along with Rigid 10K and Tullomer™. A comparison between machined and 3D-printed parts demonstrated that challenges such as porosity and surface roughness showed not to be a cause of great concern. • Ultra-high vacuum compatible 3D-printed plastics. • 3D-printed versus machined PEEK, vacuum compatibility comparison. • Outgassing properties of FDM and SLA printed materials assessed. • Low outgassing polymers: PEEK, Rigid 10K, COC, and Tullomer™.

VacuumVol. 233
Lund University (SE), MAX IV Laboratory (SE)
VINNOVA, Svenska Forskningsrådet Formas, Lunds Universitet, Vetenskapsrådet
Openalex Percentile: Top 32%
Additive Manufacturing and 3D Printing Technologies
0.61
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