Use of Real‐Time In‐Situ UV‐vis Spectrophotometry as a Tool for Monitoring Electrochemically‐Mediated Organic Synthesis

Abstract A real‐time in‐situ UV‐vis reaction monitoring tool is used for the optimization and substrate screening of two electrochemically‐mediated reactions, namely the dehydrogenation of 1,2‐diphenylhydrazines, and the hydrogenation of azobenzenes. Key reaction parameters were assayed easily and effectively, this enabling rapid optimization and substrate screening.

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Publication Details

Journal
European Journal of Organic Chemistry
Published
2024-12-23
DOI
https://doi.org/10.1002/ejoc.202401266
Primary Topic
Radical Photochemical Reactions
Type
article
Field-Weighted Citation Impact
0.00

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article

Use of Real‐Time In‐Situ UV‐vis Spectrophotometry as a Tool for Monitoring Electrochemically‐Mediated Organic Synthesis

Chelsea M. Schroeder, Nicholas E. Leadbeater
1 links
European Journal of Organic Chemistry
Radical Photochemical Reactions
article

Use of Real‐Time In‐Situ UV‐vis Spectrophotometry as a Tool for Monitoring Electrochemically‐Mediated Organic Synthesis

Chelsea M. Schroeder, Nicholas E. Leadbeater
article en

Abstract

Abstract A real‐time in‐situ UV‐vis reaction monitoring tool is used for the optimization and substrate screening of two electrochemically‐mediated reactions, namely the dehydrogenation of 1,2‐diphenylhydrazines, and the hydrogenation of azobenzenes. Key reaction parameters were assayed easily and effectively, this enabling rapid optimization and substrate screening.

European Journal of Organic ChemistryVol. 28(8)
University of Connecticut (US)
University of Connecticut
Openalex Percentile: Top 82%
Radical Photochemical Reactions
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