Bleaching Pre-Treatment of Oil Palm Empty Fruit Bunch for Nanocellulose Extraction

Oil palm empty fruit bunch (OPEFB) is one of the waste by-products when palm oil is produced. Although a waste product, it can be turned into a valuable product by extracting nanocellulose through acid hydrolysis. The process requires a few steps; the most important is the pre-treatment process. In this research, bleaching pretreatment was used to characterize empty oil palm fruit bunches as raw materials for hydrolysis reactions to extract nanocellulose. The bleaching process was done using H 2 O 2 and the resulting samples were characterized using FT-IR and SEM. FT-IR analysis revealed that lignin-associated carbonyl groups were removed and there was a decrease in hemicellulose-related acetyl group peaks which confirmed effective pre-treatment. According to Scanning Electron Microscopy (SEM), surface morphology has also changed where the bleached fibres exhibited a rougher surface than the ones that were not bleached. Bleaching is proven to be successful at removing surface impurities, hemicellulose, and lignin and isolating the cellulose for the acid hydrolysis process.

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Publication Details

Journal
Materials science forum
Published
2024-12-23
DOI
https://doi.org/10.4028/p-j7d3rh
Primary Topic
Advanced Cellulose Research Studies
Type
article
Field-Weighted Citation Impact
0.00
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article

Bleaching Pre-Treatment of Oil Palm Empty Fruit Bunch for Nanocellulose Extraction

Norhaniza Yusof, Farhana Aziz, Ahmad Fauzi Ismail, T. Ram et al.
Materials science forum
Advanced Cellulose Research Studies
article

Bleaching Pre-Treatment of Oil Palm Empty Fruit Bunch for Nanocellulose Extraction

Norhaniza Yusof, Farhana Aziz, Ahmad Fauzi Ismail, T. Ram, Woei Jye Lau
article en

Abstract

Oil palm empty fruit bunch (OPEFB) is one of the waste by-products when palm oil is produced. Although a waste product, it can be turned into a valuable product by extracting nanocellulose through acid hydrolysis. The process requires a few steps; the most important is the pre-treatment process. In this research, bleaching pretreatment was used to characterize empty oil palm fruit bunches as raw materials for hydrolysis reactions to extract nanocellulose. The bleaching process was done using H 2 O 2 and the resulting samples were characterized using FT-IR and SEM. FT-IR analysis revealed that lignin-associated carbonyl groups were removed and there was a decrease in hemicellulose-related acetyl group peaks which confirmed effective pre-treatment. According to Scanning Electron Microscopy (SEM), surface morphology has also changed where the bleached fibres exhibited a rougher surface than the ones that were not bleached. Bleaching is proven to be successful at removing surface impurities, hemicellulose, and lignin and isolating the cellulose for the acid hydrolysis process.

Materials science forumVol. 1142
University of Technology Malaysia (MY)
Openalex Percentile: Top 88%
Advanced Cellulose Research Studies
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