A fully contained sample holder capable of electron-yield detection at soft X-ray energies

A holder has been developed that enables electron yield-detected soft X-ray spectroscopy of fully contained samples at low temperature. Crucially, this design uses elements of the sample containment to collect ejected electrons, removing the need to expose samples directly to the vacuum environment of the spectrometer. The design is modular and should be adaptable to a number of different endstation configurations, enabling spectroscopy of air-sensitive, radioactive and vacuum-sensitive (biological) samples.

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Publication Details

Journal
Journal of Synchrotron Radiation
Published
2024-12-20
DOI
https://doi.org/10.1107/s1600577524011354
Primary Topic
X-ray Spectroscopy and Fluorescence Analysis
Type
article
Field-Weighted Citation Impact
0.00

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article

A fully contained sample holder capable of electron-yield detection at soft X-ray energies

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Journal of Synchrotron Radiation
X-ray Spectroscopy and Fluorescence Analysis
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A fully contained sample holder capable of electron-yield detection at soft X-ray energies

Jacob A. Branson, Stefan G. Minasian, Patrick W. Smith, Alexander S. Ditter, David K. Shuh, Bianca Schacherl, Alpha T. N’Diaye, Sebastian Günther
article en

Abstract

A holder has been developed that enables electron yield-detected soft X-ray spectroscopy of fully contained samples at low temperature. Crucially, this design uses elements of the sample containment to collect ejected electrons, removing the need to expose samples directly to the vacuum environment of the spectrometer. The design is modular and should be adaptable to a number of different endstation configurations, enabling spectroscopy of air-sensitive, radioactive and vacuum-sensitive (biological) samples.

Journal of Synchrotron RadiationVol. 32(1)
Lawrence Berkeley National Laboratory (US)
U.S. Department of Energy, Office of Science, Basic Energy Sciences, Lawrence Berkeley National Laboratory
Affordable and clean energy
Openalex Percentile: Top 67%
X-ray Spectroscopy and Fluorescence Analysis
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