Bis(N-Alkyl-N-diphenylphosphinylmethyl)diglycolamides: Synthesis and NMR Spectroscopy Study
Bis(N-Alkyl-N-diphenylphosphinylmethyl)diglycolamides [Ph2P(O)CH2N(R)C(O)CH2]2O, where R = Et, i-Pr, n-Bu, i-Bu, n-Oct, were synthesized by reaction of diglycolyl chloride with N-alkyl-N-(diphenylphosphinylmethyl)amines Ph2P(O)CH2NHR obtained by the Kabachnik–Fields reaction of aminomethylation of diphenylphosphinous acid, and their hydrochlorides. The structure of the obtained compounds was studied by 1H, 13C and 31P NMR spectroscopy.
Authors
- Kseniia V. Tcarkova (ORCID: https://orcid.org/0000-0001-8730-0521)
- Elena V. Sharova (ORCID: https://orcid.org/0000-0001-5428-596X)
- Natalia A. Bondarenko (ORCID: https://orcid.org/0000-0002-6704-6957)
- Аlexander S. Peregudov (ORCID: https://orcid.org/0000-0001-6223-0184)
- Оleg I. Аrtyushin (ORCID: https://orcid.org/0000-0001-6333-5973)
Institutions
- Kurchatov Institute (RU)
- A. N. Nesmeyanov Institute of Organoelement Compounds (RU)
Publication Details
- Journal
- Журнал Общей Химии
- Published
- 2024-12-20
- DOI
- https://doi.org/10.31857/s0044460x24070046
- Primary Topic
- Radioactive element chemistry and processing
- Type
- article
- Field-Weighted Citation Impact
- 0.00