Selection of Conditions for Alkylation of 3-Amino-1,2,4-triazole
In this work the alkylation of 3-amino-1,2,4-triazole with dichloroethane under phase-transfer catalysis conditions was studied. Synthesis conditions were selected. The structure of 1N-(2-chloroethyl)-3-amino-1,2,4-triazole was proven by IR, 1H, 13C and 2D HSQC NMR spectroscopy, gas chromatography-mass spectrometry and X-ray diffraction.
Authors
- Ekaterina A. Petukhova (ORCID: https://orcid.org/0000-0002-0776-4041)
- Е. А. Данилова (ORCID: https://orcid.org/0000-0001-6765-6707)
- М. В. Дмитриев (ORCID: https://orcid.org/0000-0002-8817-0543)
Institutions
- Perm State University (RU)
- Ivanovo State University of Chemistry and Technology (RU)
Publication Details
- Journal
- Russian Journal of General Chemistry
- Published
- 2024-11-01
- DOI
- https://doi.org/10.1134/s1070363224110045
- Primary Topic
- Chemical Synthesis and Analysis
- Type
- article
- Field-Weighted Citation Impact
- 0.00