Sonochemical synthesis of spine-type СuMn2O4 nanomaterial

Spinel-type CuMn2O4 nanomaterial particles were synthesized by co-precipitation in an ultrasonic cavitation field. Based on the results of X-ray diffraction, the theoretical density (5 548 kg/m3) of CuMn2O4 spinel with a cubic structure and the average crystallite size, which was ~21 nm, were calculated. The elemental composition and functional groups of chemical bonds of the synthesized material were identified, respectively, by the methods of energy dispersive X-ray analysis and IR spectroscopy with Fourier transform. Using the method of scanning electron microscopy, it was established that CuMn2O4 spinel particles have a quasi-spherical shape and are prone to slight agglomeration.

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Publication Details

Journal
Chemistry Technology and Application of Substances
Published
2024-12-01
DOI
https://doi.org/10.23939/ctas2024.02.035
Primary Topic
Catalysis and Oxidation Reactions
Type
article
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article

Sonochemical synthesis of spine-type СuMn2O4 nanomaterial

Yu. V. Sukhatskyi, V. V. Tsymbaliuk
Chemistry Technology and Application of Substances
Catalysis and Oxidation Reactions
article

Sonochemical synthesis of spine-type СuMn2O4 nanomaterial

Yu. V. Sukhatskyi, V. V. Tsymbaliuk
article en

Abstract

Spinel-type CuMn2O4 nanomaterial particles were synthesized by co-precipitation in an ultrasonic cavitation field. Based on the results of X-ray diffraction, the theoretical density (5 548 kg/m3) of CuMn2O4 spinel with a cubic structure and the average crystallite size, which was ~21 nm, were calculated. The elemental composition and functional groups of chemical bonds of the synthesized material were identified, respectively, by the methods of energy dispersive X-ray analysis and IR spectroscopy with Fourier transform. Using the method of scanning electron microscopy, it was established that CuMn2O4 spinel particles have a quasi-spherical shape and are prone to slight agglomeration.

Chemistry Technology and Application of SubstancesVol. 7(2)
Affordable and clean energy
Openalex Percentile: Top 89%
Catalysis and Oxidation Reactions
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