Utilizing controlled hydrogen-assisted pre-cracking to assess the fracture toughness of high-strength steels
• Hydrogen-assisted cracking is presented as an alternative method to fatigue cracking in fracture mechanics tests. • Hydrogen-assisted pre-cracking improves CNT specimen use in fracture mechanics tests. • Hydrogen extraction at 573 K recommended for accurate fracture toughness testing after hydrogen pre-cracking. • Subcritical crack growth occurs in specimens heat-treated at 473 K due to hydrogen trapped at boundaries. • Fracture toughness in the presence of hydrogen decreases with increasing hydrogen pre-charging duration. The controlled initiation of detectable cracks is pivotal in fracture mechanics investigations. Typically, pre-notched specimens are utilized, and fatigue cracks are induced at the notch root. In the specific case of circumferentially notched tensile (CNT) specimens, fatigue cracks originate from rotating bending. Subsequently, the fatigue pre-cracked specimens undergo tensional fracture, and fracture toughness is ascertained based on the crack length and fracture stress. However, a notable portion of fatigue cracks initiated in this manner exhibits non-uniform radial lengths, leading to a ligament eccentricity relative to the fracture surface centre. Consequently, accounting for bending stresses alongside tensile stresses becomes imperative, which makes fracture mechanics testing methods more complex. In a previous study, the authors demonstrated that hydrogen-assisted cracking (HAC) can yield highly symmetric circumferential cracks in CNT specimens of high-strength quenched-tempered steel. In this context, the consistent circumferential formation of the crack, as well as the radial crack length are regulated by both the duration of hydrogen pre-charging and the subsequently applied preload. This paper elucidates the utility of hydrogen-induced circumferential cracks for evaluating fracture toughness. Both the fracture toughness in the presence of hydrogen ( K Ic H ) and the fracture toughness without the influence of hydrogen ( K Ic ) are assessed reliably. For the latter, a hydrogen extraction heat treatment is carried out and the influence of the extraction temperature is discussed. By following this method, fracture toughness of CNT specimens can be reliably determined with simplicity, eliminating the need to consider bending stresses. This significantly enhances the usability of CNT specimens in fracture mechanics testing, which is why hydrogen-assisted pre-cracking is seen as a promising alternative to the established fatigue pre-cracking.
Authors
- D. Damyanov
- Holger Hoche (ORCID: https://orcid.org/0000-0002-5396-7202)
- Marcus Klein (ORCID: https://orcid.org/0000-0001-5875-9472)
- Matthias Oechsner (ORCID: https://orcid.org/0000-0003-0248-4232)
- Michael Brilz (ORCID: https://orcid.org/0009-0003-2030-0668)
- M Szabo
- Anutsara Chakamnan
Institutions
- Technische Universität Darmstadt (DE)
Publication Details
- Journal
- Engineering Fracture Mechanics
- Published
- 2024-12-12
- DOI
- https://doi.org/10.1016/j.engfracmech.2024.110742
- Citations
- 2
- Primary Topic
- Hydrogen embrittlement and corrosion behaviors in metals
- Type
- article
- Field-Weighted Citation Impact
- 0.34
Funders
- AiF Projekt