On the effect of precession for magnetic differential phase contrast imaging

The separation of diffraction effects from phase contrast is a major challenge for differential phase contrast (DPC) imaging in scanning transmission electron microscopy (STEM). The application of electron beam precession has previously been proven successful in homogenizing the direct beam and improving the imaging of both long-range electric and magnetic fields. However, magnetic STEM-DPC imaging performed in a low magnification (LM) STEM mode suffers from significant aberrations of the probe forming lens and the consequent impediment of small precession angles. By investigating the application of precession path segmentation to LM-STEM precessed scans for the imaging of LSMO and FeAl thin film samples, the initially reported benefits of precession were discovered to be less substantial than originally assumed. The segmentation methodology reveals that precession induced beam phase shifts account for a large part of the DPC induction profile smoothing, and the precession path is non-circular, leading to streaking artifacts in the reconstructed induction maps.

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Publication Details

Journal
Micron
Published
2024-12-04
DOI
https://doi.org/10.1016/j.micron.2024.103761
Primary Topic
Advanced X-ray Imaging Techniques
Type
article
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article

On the effect of precession for magnetic differential phase contrast imaging

Daesung Park, Nini Pryds, Felix Trier, Gregory Nordahl et al.
Micron
Advanced X-ray Imaging Techniques
article

On the effect of precession for magnetic differential phase contrast imaging

Daesung Park, Nini Pryds, Felix Trier, Gregory Nordahl, Magnus Nord, Sivert Dagenborg, Jørgen Sørhaug, Eric Brand, Andrea D’Alessio, Nikolas Vitaliti
article en

Abstract

The separation of diffraction effects from phase contrast is a major challenge for differential phase contrast (DPC) imaging in scanning transmission electron microscopy (STEM). The application of electron beam precession has previously been proven successful in homogenizing the direct beam and improving the imaging of both long-range electric and magnetic fields. However, magnetic STEM-DPC imaging performed in a low magnification (LM) STEM mode suffers from significant aberrations of the probe forming lens and the consequent impediment of small precession angles. By investigating the application of precession path segmentation to LM-STEM precessed scans for the imaging of LSMO and FeAl thin film samples, the initially reported benefits of precession were discovered to be less substantial than originally assumed. The segmentation methodology reveals that precession induced beam phase shifts account for a large part of the DPC induction profile smoothing, and the precession path is non-circular, leading to streaking artifacts in the reconstructed induction maps.

MicronVol. 190
Norwegian University of Science and Technology (NO), Technical University of Denmark (DK)
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Openalex Percentile: Top 69%
Advanced X-ray Imaging Techniques
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On the effect of precession for magnetic differential phase contrast imaging — Daesung Park, Nini Pryds, et al. · Micron (2024) | TGRS Research Map | TGRS