Evolution of Microstructure during Creep Deformation in a Forged 617 Superalloy

Creep tests are conducted on forged 617 M superalloy samples at 650, 700, and 750 °C at stresses ranging from 115 to 320 MPa. At 650 °C, a significant steady‐state secondary creep is observed, while at 700 and 750 °C limited secondary creep and prolonged tertiary creep are observed. Creep data analysis using power‐law creep approach estimates high‐stress exponents ( n ≈ 13.4 at 650 °C, ≈11.5 at 700 °C, and ≈9.7 at 750 °C) and activation energy ( Q ≈ 530.6 kJ mole −1 ). After incorporating threshold stress, the activation energy for creep is found to be ≈261 kJ mole −1 . This is consistent with the activation energy for lattice self‐diffusion in the alloy. Transmission electron microscopy provides evidences affirming that climb‐controlled dislocation creep may be the operative creep mechanism. Ni 3 (Al, Ti) (γ′) precipitates and M 23 C 6 carbides evolve during exposure at operating temperatures. These are observed to lead to enhanced creep resistance at 700 °C. Significant coarsening rate of γ′ precipitates are noted during exposure at 750 °C. This intensifies recovery processes and lowers creep threshold stress drastically. Extended tertiary creep prevails near the service conditions of this alloy, which is ascribed to instability in microstructure during creep.

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Journal
Advanced Engineering Materials
Published
2024-11-27
DOI
https://doi.org/10.1002/adem.202401983
Citations
3
Primary Topic
High Temperature Alloys and Creep
Type
article
Field-Weighted Citation Impact
0.64
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article

Evolution of Microstructure during Creep Deformation in a Forged 617 Superalloy

Ujjwal Prakash, Pankaj Rawat, Ratnakar Singh, Sajad Hamid
3 citations
Advanced Engineering Materials
High Temperature Alloys and Creep
0.64
article

Evolution of Microstructure during Creep Deformation in a Forged 617 Superalloy

Ujjwal Prakash, Pankaj Rawat, Ratnakar Singh, Sajad Hamid
article en
3 citations

Abstract

Creep tests are conducted on forged 617 M superalloy samples at 650, 700, and 750 °C at stresses ranging from 115 to 320 MPa. At 650 °C, a significant steady‐state secondary creep is observed, while at 700 and 750 °C limited secondary creep and prolonged tertiary creep are observed. Creep data analysis using power‐law creep approach estimates high‐stress exponents ( n ≈ 13.4 at 650 °C, ≈11.5 at 700 °C, and ≈9.7 at 750 °C) and activation energy ( Q ≈ 530.6 kJ mole −1 ). After incorporating threshold stress, the activation energy for creep is found to be ≈261 kJ mole −1 . This is consistent with the activation energy for lattice self‐diffusion in the alloy. Transmission electron microscopy provides evidences affirming that climb‐controlled dislocation creep may be the operative creep mechanism. Ni 3 (Al, Ti) (γ′) precipitates and M 23 C 6 carbides evolve during exposure at operating temperatures. These are observed to lead to enhanced creep resistance at 700 °C. Significant coarsening rate of γ′ precipitates are noted during exposure at 750 °C. This intensifies recovery processes and lowers creep threshold stress drastically. Extended tertiary creep prevails near the service conditions of this alloy, which is ascribed to instability in microstructure during creep.

Advanced Engineering MaterialsVol. 27(1)
Indian Institute of Technology Roorkee (IN)
Affordable and clean energy
Openalex Percentile: Top 34%
High Temperature Alloys and Creep
0.64
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Evolution of Microstructure during Creep Deformation in a Forged 617 Superalloy — Ujjwal Prakash, Pankaj Rawat, et al. · Advanced Engineering Materials (2024) | TGRS Research Map | TGRS