<i>RAPID</i>: an <i>ImageJ</i> macro for indexing electron diffraction zone axis spot patterns of cubic materials

As an extension to previous work, the <i>ImageJ</i> macro script <i>RAPID</i> (ratio-method pattern indexing) has been developed to allow instant indexing of calibrated and uncalibrated zone axis aligned electron diffraction patterns of cubic lattices using the <i>R<sub>n</sub></i> ratio principle. The program can be used to index zone axis aligned selected-area electron diffraction patterns, nanobeam electron diffraction patterns, transmission electron microscopy (TEM) Kikuchi patterns and even fast Fourier transforms of high-resolution (scanning) TEM images. The program allows the user to quickly assess whether the material under investigation belongs to the cubic crystal system, is pseudo-cubic or is not cubic at all by adjusting the boundary parameters and allowed errors for lattice indexing. The software also allows one to distinguish between the <i>P</i>, <i>I</i> and <i>F</i> Bravais lattices for certain zone axis directions. For calibrated diffraction patterns, the lattice parameters can be obtained, allowing verification of the material under investigation or phase identification in connection with a structural database. In addition, the program can be employed for determination or verification of the used instrument's camera constant when reference materials are used. Therefore, it is a convenient tool for on-site crystallographic analysis in TEM laboratories.

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Publication Details

Journal
Journal of Applied Crystallography
Published
2024-11-26
DOI
https://doi.org/10.1107/s1600576724010215
Citations
3
Primary Topic
X-ray Diffraction in Crystallography
Type
article
Field-Weighted Citation Impact
0.35

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article

RAPID: an ImageJ macro for indexing electron diffraction zone axis spot patterns of cubic materials

Thomas E. Weirich
3 citations
Journal of Applied Crystallography
X-ray Diffraction in Crystallography
0.35
article

RAPID: an ImageJ macro for indexing electron diffraction zone axis spot patterns of cubic materials

Thomas E. Weirich
article en
3 citations

Abstract

As an extension to previous work, the <i>ImageJ</i> macro script <i>RAPID</i> (ratio-method pattern indexing) has been developed to allow instant indexing of calibrated and uncalibrated zone axis aligned electron diffraction patterns of cubic lattices using the <i>R<sub>n</sub></i> ratio principle. The program can be used to index zone axis aligned selected-area electron diffraction patterns, nanobeam electron diffraction patterns, transmission electron microscopy (TEM) Kikuchi patterns and even fast Fourier transforms of high-resolution (scanning) TEM images. The program allows the user to quickly assess whether the material under investigation belongs to the cubic crystal system, is pseudo-cubic or is not cubic at all by adjusting the boundary parameters and allowed errors for lattice indexing. The software also allows one to distinguish between the <i>P</i>, <i>I</i> and <i>F</i> Bravais lattices for certain zone axis directions. For calibrated diffraction patterns, the lattice parameters can be obtained, allowing verification of the material under investigation or phase identification in connection with a structural database. In addition, the program can be employed for determination or verification of the used instrument's camera constant when reference materials are used. Therefore, it is a convenient tool for on-site crystallographic analysis in TEM laboratories.

Journal of Applied CrystallographyVol. 57(6)
RWTH Aachen University (DE)
Deutsche Forschungsgemeinschaft
Openalex Percentile: Top 43%
X-ray Diffraction in Crystallography
0.35
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