Processing TiC nanoparticle reinforced aluminum matrix composites in PBF-LB: Powder blending approach, particle sintering, precipitation and grain refinement

• PBF-LB combined with a blending approach works to build AlSi7Mg0.6 + TiC composites. • Blending and printing reduce total TiC nanoparticle content. • TiC partially dissolved and precipitates Al 3 Ti. • Al 3 Ti precipitates are relevant for grain refinement. • Sintering of TiC nanoparticle agglomerates during PBF-LB. Particle-reinforced aluminum-matrix-composites (AMCs) promise enhanced mechanical properties while maintaining the lightweight potential of aluminum. Fabricating AMCs near-net-shape is desirable because it avoids the drawback of the difficult machining. Laser powder bed fusion (PBF-LB) has the potential to achieve this goal. An economically attractive powder blending approach was used to modify AlSi7Mg0.6 powder with TiC nanoparticles. The resulting blend was processed in a PBF-LB machine to fabricate AMCs. This paper shows how to maximize the grain refinement potential of TiC nanoparticles by using a high mixing time of 1215 min to break up agglomerates. For a better understanding of the process related microstructure, investigations of the TiC distribution in blend and composites have been conducted by SEM and EDS. The formation of TiC microparticles formed by sintering of agglomerates are an integral part of the final microstructure. Measuring the overall carbon content of the specimens reveals a loss of TiC during PBF-LB. The root causes are discussed in terms of agglomeration and smoke generation and countermeasures are proposed. The presented approach is an effective way to introduce nanoparticles and to refine the microstructure. It can also be adapted to other material systems to modify the grain size and reduce the texture.

Authors

Institutions

Publication Details

Journal
Materials & Design
Published
2024-11-26
DOI
https://doi.org/10.1016/j.matdes.2024.113490
Citations
12
Primary Topic
Aluminum Alloys Composites Properties
Type
article
Field-Weighted Citation Impact
2.55
Controls
|||
ALL TIME
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
article

Processing TiC nanoparticle reinforced aluminum matrix composites in PBF-LB: Powder blending approach, particle sintering, precipitation and grain refinement

Eric A. Jägle, Raphael Freundl
12 citations
Materials & Design
Aluminum Alloys Composites Properties
2.55
article

Processing TiC nanoparticle reinforced aluminum matrix composites in PBF-LB: Powder blending approach, particle sintering, precipitation and grain refinement

Eric A. Jägle, Raphael Freundl
article en
12 citations

Abstract

• PBF-LB combined with a blending approach works to build AlSi7Mg0.6 + TiC composites. • Blending and printing reduce total TiC nanoparticle content. • TiC partially dissolved and precipitates Al 3 Ti. • Al 3 Ti precipitates are relevant for grain refinement. • Sintering of TiC nanoparticle agglomerates during PBF-LB. Particle-reinforced aluminum-matrix-composites (AMCs) promise enhanced mechanical properties while maintaining the lightweight potential of aluminum. Fabricating AMCs near-net-shape is desirable because it avoids the drawback of the difficult machining. Laser powder bed fusion (PBF-LB) has the potential to achieve this goal. An economically attractive powder blending approach was used to modify AlSi7Mg0.6 powder with TiC nanoparticles. The resulting blend was processed in a PBF-LB machine to fabricate AMCs. This paper shows how to maximize the grain refinement potential of TiC nanoparticles by using a high mixing time of 1215 min to break up agglomerates. For a better understanding of the process related microstructure, investigations of the TiC distribution in blend and composites have been conducted by SEM and EDS. The formation of TiC microparticles formed by sintering of agglomerates are an integral part of the final microstructure. Measuring the overall carbon content of the specimens reveals a loss of TiC during PBF-LB. The root causes are discussed in terms of agglomeration and smoke generation and countermeasures are proposed. The presented approach is an effective way to introduce nanoparticles and to refine the microstructure. It can also be adapted to other material systems to modify the grain size and reduce the texture.

Materials & DesignVol. 248
Universität der Bundeswehr München (DE)
Openalex Percentile: Top 10%
Aluminum Alloys Composites Properties
2.55
AI Navigator

Ask Laika to Summarize, Analyze, and Connect papers live on the map.

Summarize Papers & Methodologies

Extract key findings, datasets, and comparative methods across publications.

Benchmark Rankings & Visual Analytics

Rank top research institutions, authors, funders, topics, and journals by Field-Weighted Citation Impact (FWCI) and paper volume with instant charts.

Connect Distant Disciplines

Bridge topological clusters on the map to find hidden collaborative intersections.

Processing TiC nanoparticle reinforced aluminum matrix composites in PBF-LB: Powder blending approach, particle sintering, precipitation and grain refinement — Eric A. Jägle, Raphael Freundl · Materials & Design (2024) | TGRS Research Map | TGRS