Glass Microwave Microfluidic Devices for Broadband Characterization of Diverse Fluids

We demonstrate a glass microwave microfluidic device for determining the permittivity of a wide range of liquid chemicals from 100 MHz to 30 GHz with associated uncertainties. Conventional microwave microfluidic devices use polymer-based microfluidic layers for fluid delivery, but these polymers swell in organic solvents and are not suitable for many applications. Our device incorporates glass microfluidic channels with platinum coplanar waveguides (CPWs) to provide a solvent-resistant architecture for broadband dielectric spectroscopy. We utilize broadband scattering parameter measurements with a vector network analyzer (VNA) on a wafer probing station and multiline thru-reflect-line (mTRL) calibrations to extract the distributed circuit parameters of transmission lines and solve for fluid permittivity. In this work, we demonstrate the utility of the device by measuring the permittivity of four organic solvents difficult to measure otherwise: hexane, heptane, decane, and toluene.

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Publication Details

Journal
IEEE Transactions on Microwave Theory and Techniques
Published
2024-11-15
DOI
https://doi.org/10.1109/tmtt.2024.3491653
Citations
2
Primary Topic
Microwave and Dielectric Measurement Techniques
Type
article
Field-Weighted Citation Impact
0.42

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article

Glass Microwave Microfluidic Devices for Broadband Characterization of Diverse Fluids

Nathan D. Orloff, James C. Booth, Christian J. Long, Tomasz M. Karpisz et al.
2 citations
IEEE Transactions on Microwave Theory and Techniques
Microwave and Dielectric Measurement Techniques
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article

Glass Microwave Microfluidic Devices for Broadband Characterization of Diverse Fluids

Nathan D. Orloff, James C. Booth, Christian J. Long, Tomasz M. Karpisz, Bryan T. Bosworth, Nicholas Derimow, Jacob T. Pawlik, Angela C. Stelson, Sarah R. Evans, Yasaman Kazemipour
article en
2 citations

Abstract

We demonstrate a glass microwave microfluidic device for determining the permittivity of a wide range of liquid chemicals from 100 MHz to 30 GHz with associated uncertainties. Conventional microwave microfluidic devices use polymer-based microfluidic layers for fluid delivery, but these polymers swell in organic solvents and are not suitable for many applications. Our device incorporates glass microfluidic channels with platinum coplanar waveguides (CPWs) to provide a solvent-resistant architecture for broadband dielectric spectroscopy. We utilize broadband scattering parameter measurements with a vector network analyzer (VNA) on a wafer probing station and multiline thru-reflect-line (mTRL) calibrations to extract the distributed circuit parameters of transmission lines and solve for fluid permittivity. In this work, we demonstrate the utility of the device by measuring the permittivity of four organic solvents difficult to measure otherwise: hexane, heptane, decane, and toluene.

IEEE Transactions on Microwave Theory and TechniquesVol. 73(1)
National Institute of Standards and Technology (US)
National Institute of Standards and Technology
Affordable and clean energy
Openalex Percentile: Top 37%
Microwave and Dielectric Measurement Techniques
0.42
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