Synthesis and Structure of Ethyl 4-Aryl-2-oxo-2,3,4,10-tetrahydrobenzo[4,5]imidazo[1,2-<i>a</i>]pyrimidine-3-carboxylates

Ethyl 4-aryl-2-oxo-2,3,4,10-tetrahydrobenzo[4,5]imidazo[1,2-a]pyrimidine-3-carboxylates were prepared by three-component one-pot condensation of diethylmalonate, aromatic aldehyde, 2-aminobenzimidazole in ethanol in the presence of piperidine. The structure of the obtained compounds was determined by 1H, 13С NMR spectroscopy and single crystal X-ray diffraction analysis.

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Journal
Журнал Общей Химии
Published
2024-11-13
DOI
https://doi.org/10.31857/s0044460x24060034
Primary Topic
Synthesis of heterocyclic compounds
Type
article
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article

Synthesis and Structure of Ethyl 4-Aryl-2-oxo-2,3,4,10-tetrahydrobenzo[4,5]imidazo[1,2-a]pyrimidine-3-carboxylates

М. В. Дмитриев, N. V. Slepova, Т. М. Замараева, K. V. Podchezertseva
Журнал Общей Химии
Synthesis of heterocyclic compounds
article

Synthesis and Structure of Ethyl 4-Aryl-2-oxo-2,3,4,10-tetrahydrobenzo[4,5]imidazo[1,2-a]pyrimidine-3-carboxylates

М. В. Дмитриев, N. V. Slepova, Т. М. Замараева, K. V. Podchezertseva
article en

Abstract

Ethyl 4-aryl-2-oxo-2,3,4,10-tetrahydrobenzo[4,5]imidazo[1,2-a]pyrimidine-3-carboxylates were prepared by three-component one-pot condensation of diethylmalonate, aromatic aldehyde, 2-aminobenzimidazole in ethanol in the presence of piperidine. The structure of the obtained compounds was determined by 1H, 13С NMR spectroscopy and single crystal X-ray diffraction analysis.

Журнал Общей ХимииVol. 94(6)
Moscow Power Engineering Institute (RU), Ministry of Health of the Russian Federation (RU), Solikamsk State Pedagogical Institute (RU), Perm State Pharmaceutical Academy (RU)
Clean water and sanitation
Openalex Percentile: Top 85%
Synthesis of heterocyclic compounds
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