Solution combustion synthesis for rare earth nano metal oxides using D-glycine as fuel: morphological and optical studies

Abstract Three different nano rate earth oxides, i.e. CeO 2, La 2 O 3, and ThO 2 have been prepared through solution combustion synthesis method using Cerous Nitrate Hexahydrate, Lanthanum Hexahydrate, and Thorium Nitrate as an oxidizer, respectively and glycine as a fuel. The synthesized nano powder was characterized by powder diffraction (PXRD), FTIR, Scanning Electron Microscopy (SEM), UV–vis Diffuse Reflectance Spectrum (UV–vis DRS), and Energy dispersive x-ray spectroscopy (EDX). CeO 2, La 2 O 3, and ThO 2 possess Cubic, Hexagonal and Cubic phases respectively. Morphological results showed the stable and sponge-like surface of each specimen. The optical band gap of CeO 2 , La 2 O 3, and ThO 2 obtained from Tauc Plots ranges 3.10 eV, 4.84 eV and 5.76 eV which shows interesting behavior and hence six Refractive Indices modeling has been applied to optimize the parameter to utilize these rare earth metal oxides in the solar reflector system using appropriate matrix.

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Publication Details

Journal
Physica Scripta
Published
2024-11-08
DOI
https://doi.org/10.1088/1402-4896/ad9099
Citations
4
Primary Topic
Catalytic Processes in Materials Science
Type
article
Field-Weighted Citation Impact
0.47
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Solution combustion synthesis for rare earth nano metal oxides using D-glycine as fuel: morphological and optical studies

B. S. Madhukar, Ashish R. Tanna, Dhara Maheta
4 citations
Physica Scripta
Catalytic Processes in Materials Science
0.47
article

Solution combustion synthesis for rare earth nano metal oxides using D-glycine as fuel: morphological and optical studies

B. S. Madhukar, Ashish R. Tanna, Dhara Maheta
article en
4 citations

Abstract

Abstract Three different nano rate earth oxides, i.e. CeO 2, La 2 O 3, and ThO 2 have been prepared through solution combustion synthesis method using Cerous Nitrate Hexahydrate, Lanthanum Hexahydrate, and Thorium Nitrate as an oxidizer, respectively and glycine as a fuel. The synthesized nano powder was characterized by powder diffraction (PXRD), FTIR, Scanning Electron Microscopy (SEM), UV–vis Diffuse Reflectance Spectrum (UV–vis DRS), and Energy dispersive x-ray spectroscopy (EDX). CeO 2, La 2 O 3, and ThO 2 possess Cubic, Hexagonal and Cubic phases respectively. Morphological results showed the stable and sponge-like surface of each specimen. The optical band gap of CeO 2 , La 2 O 3, and ThO 2 obtained from Tauc Plots ranges 3.10 eV, 4.84 eV and 5.76 eV which shows interesting behavior and hence six Refractive Indices modeling has been applied to optimize the parameter to utilize these rare earth metal oxides in the solar reflector system using appropriate matrix.

Physica ScriptaVol. 99(12)
RK University (IN), JSS Science and Technology University (IN)
Openalex Percentile: Top 38%
Catalytic Processes in Materials Science
0.47
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