Preparation and Characterization of Mechanical Properties of HAP/45S5 Bioglass Laminated Ceramic Composites via Spark Plasma Sintering

Hydroxyapatite (HAP) displays a high degree of similarity to the inorganic components that make up roughly 70% of human hard tissue, and it possesses exceptional biological activity and biocompatibility. It is currently internationally recognized as the most biologically active hard tissue implant material. However, its substandard mechanical properties have significantly limited the application of HAP in areas requiring load bearing or in the repair of large bone defects. In this study, HAP/45S5 bioglass laminated ceramic composites were consolidated using the spark plasma sintering (SPS) technique. The grain growth and phase transformation of HAP and 45S5 bioglass were examined at various sintering temperatures. The mechanical properties of the laminated composites were investigated. At 950 °C, the flexural strength and fracture work of the sintered body were (153.22 ± 7.7) MPa and (2049 ± 34) J·m<sup>-2</sup>, respectively. These results corresponded to the load-displacement curves and showed that the composites met the mechanical performance requirements of the support material.

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Publication Details

Journal
Materials
Published
2024-11-06
DOI
https://doi.org/10.3390/ma17225413
Citations
2
Primary Topic
Bone Tissue Engineering Materials
Type
article
Field-Weighted Citation Impact
0.37
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article

Preparation and Characterization of Mechanical Properties of HAP/45S5 Bioglass Laminated Ceramic Composites via Spark Plasma Sintering

Meng Ye, Bing Yun, Xinge Li
2 citations
Materials
Bone Tissue Engineering Materials
0.37
article

Preparation and Characterization of Mechanical Properties of HAP/45S5 Bioglass Laminated Ceramic Composites via Spark Plasma Sintering

Meng Ye, Bing Yun, Xinge Li
article en
2 citations

Abstract

Hydroxyapatite (HAP) displays a high degree of similarity to the inorganic components that make up roughly 70% of human hard tissue, and it possesses exceptional biological activity and biocompatibility. It is currently internationally recognized as the most biologically active hard tissue implant material. However, its substandard mechanical properties have significantly limited the application of HAP in areas requiring load bearing or in the repair of large bone defects. In this study, HAP/45S5 bioglass laminated ceramic composites were consolidated using the spark plasma sintering (SPS) technique. The grain growth and phase transformation of HAP and 45S5 bioglass were examined at various sintering temperatures. The mechanical properties of the laminated composites were investigated. At 950 °C, the flexural strength and fracture work of the sintered body were (153.22 ± 7.7) MPa and (2049 ± 34) J·m<sup>-2</sup>, respectively. These results corresponded to the load-displacement curves and showed that the composites met the mechanical performance requirements of the support material.

MaterialsVol. 17(22)
University of Science and Technology Beijing (CN)
Openalex Percentile: Top 42%
Bone Tissue Engineering Materials
0.37
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Preparation and Characterization of Mechanical Properties of HAP/45S5 Bioglass Laminated Ceramic Composites via Spark Plasma Sintering — Meng Ye, Bing Yun, et al. · Materials (2024) | TGRS Research Map | TGRS