Rapid sustainable synthesis of Mn2O3, CuO, and binary CuO/Mn2O3 nanoparticles using continuous laser diode for enhanced antibacterial strategy against resistant pathogens

Substantial health issues have recently resulted from the sharp rise of antibiotic-resistant bacteria. Researchers are looking for substitute antimicrobial agents to manage or stop pathogen-induced illnesses. Effective antibacterial drugs are developed using a variety of techniques, and nanoscale is definitely a promising substance in this regard. In this work, it was provided a unique quick sustainable synthesis approach of Mn 2 O 3, CuO and CuO/Mn 2 O 3 using a continuous laser diode (CLD). Manganese(II) acetate, deionized water|(DW), and sodium hydroxide (NaOH) are used to prepare a gelatinous solution of Manganese(II) hydroxide Mn(OH) 2 . A gelatinous solution of Mn(OH) 2 was poured into a circular plate and then it was bombarded by a continuous laser diode. A black powder of Mn 2 O 3 nanoparticles was obtained. The nanoparticles were characterized using various techniques such as Scanning electron microscope (SEM), transmitted electron microscope (TEM), X-ray diffraction (XRD), and Fourier-transform infrared spectroscopy (FTIR). XRD results of the MnO 2 nanoparticles show a high degree of crystallinity. The average particle size of 38 [nm] can be observed for samples prepared at time 30 min was determined by SEM and 30 nm by TEM. Mn 2 O 3, CuO and CuO/Mn 2 O 3 nanoparticles were used for decontamination and inactivation of Escherichia coli , Staphylococcus, pseudomonas and Candid strain clinical isolates as an alternative sterilization method. The Antibacterial activity shows that Mn 2 O 3 has a minimum activity while CuO and CuO/Mn 2 O 3 are more influential. The conclusion considered a new direct way to synthesize of Mn 2 O 3, CuO, and CuO/Mn 2 O 3 nanoparticles that is employed in many scientific applications.

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Publication Details

Journal
Case Studies in Chemical and Environmental Engineering
Published
2024-11-05
DOI
https://doi.org/10.1016/j.cscee.2024.101003
Citations
5
Primary Topic
Copper-based nanomaterials and applications
Type
article
Field-Weighted Citation Impact
0.59
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article

Rapid sustainable synthesis of Mn2O3, CuO, and binary CuO/Mn2O3 nanoparticles using continuous laser diode for enhanced antibacterial strategy against resistant pathogens

Ahmed Abed Anber, Ahmed Mahdi Rheima, Ammar S. Hameed, Jameel M. Dhabab
5 citations
Case Studies in Chemical and Environmental Engineering
Copper-based nanomaterials and applications
0.59
article

Rapid sustainable synthesis of Mn2O3, CuO, and binary CuO/Mn2O3 nanoparticles using continuous laser diode for enhanced antibacterial strategy against resistant pathogens

Ahmed Abed Anber, Ahmed Mahdi Rheima, Ammar S. Hameed, Jameel M. Dhabab
article en
5 citations

Abstract

Substantial health issues have recently resulted from the sharp rise of antibiotic-resistant bacteria. Researchers are looking for substitute antimicrobial agents to manage or stop pathogen-induced illnesses. Effective antibacterial drugs are developed using a variety of techniques, and nanoscale is definitely a promising substance in this regard. In this work, it was provided a unique quick sustainable synthesis approach of Mn 2 O 3, CuO and CuO/Mn 2 O 3 using a continuous laser diode (CLD). Manganese(II) acetate, deionized water|(DW), and sodium hydroxide (NaOH) are used to prepare a gelatinous solution of Manganese(II) hydroxide Mn(OH) 2 . A gelatinous solution of Mn(OH) 2 was poured into a circular plate and then it was bombarded by a continuous laser diode. A black powder of Mn 2 O 3 nanoparticles was obtained. The nanoparticles were characterized using various techniques such as Scanning electron microscope (SEM), transmitted electron microscope (TEM), X-ray diffraction (XRD), and Fourier-transform infrared spectroscopy (FTIR). XRD results of the MnO 2 nanoparticles show a high degree of crystallinity. The average particle size of 38 [nm] can be observed for samples prepared at time 30 min was determined by SEM and 30 nm by TEM. Mn 2 O 3, CuO and CuO/Mn 2 O 3 nanoparticles were used for decontamination and inactivation of Escherichia coli , Staphylococcus, pseudomonas and Candid strain clinical isolates as an alternative sterilization method. The Antibacterial activity shows that Mn 2 O 3 has a minimum activity while CuO and CuO/Mn 2 O 3 are more influential. The conclusion considered a new direct way to synthesize of Mn 2 O 3, CuO, and CuO/Mn 2 O 3 nanoparticles that is employed in many scientific applications.

Case Studies in Chemical and Environmental EngineeringVol. 10
University of Baghdad (IQ), Mustansiriyah University (IQ), University of Kerbala (IQ)
Responsible consumption and production
Openalex Percentile: Top 33%
Copper-based nanomaterials and applications
0.59
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