Effect of Homogenization Cycle on Precipitation of Dispersoids and Abnormal Grain Growth in an Al-Mg-Si Alloy

AA6xxx alloys are used for various automotive and architectural applications where microstructural characteristics are critical to have acceptable final properties. Abnormal Grain Growth (AGG) in these alloys, industrially termed as Peripheral Coarse Grain (PCG) is undesirable and Mn, Cr based non-coherent dispersoids are used to control the extent of PCG. Homogenization soaking temperature and time along with heating rates determine the size, distribution with grains and volume fraction of these dispersoids. In this study the heating rates are varied in lab and industrial setting to assess the effect of aforementioned dispersoid features using SEM and digital microscopy. It is found that higher heating rates lead to coarser and lower area fraction of dispersoids which finally results in markedly large PCG in industrial extrusion. Observed dispersoid features were described based on basic kinetics and Thermo-Calc TM predicted trends of micro-segregation, fraction of dispersoids and fraction of potential nucleating sites (β’-Mg 2 Si) of dispersoids. A static recrystallization model was used to calculate the driving and retarding pressures based on substructural (EBSD analysis) and dispersoid features (SEM+ image analysis). The predicted recrystallisation response and PCG grain size was in close agreement with the observed values. This study highlights the significance of homogenization heating rates in addition to soaking time and temperature for PCG control.

Authors

Publication Details

Journal
Materials science forum
Published
2024-10-31
DOI
https://doi.org/10.4028/p-kcuq7j
Primary Topic
Aluminum Alloy Microstructure Properties
Type
article
Field-Weighted Citation Impact
0.00

Funders

Controls
|||
ALL TIME
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
article

Effect of Homogenization Cycle on Precipitation of Dispersoids and Abnormal Grain Growth in an Al-Mg-Si Alloy

Manu Saxena, Sumit Kumar Gahlyan, Vivek Srivastava, Shavi Agrawal et al.
Materials science forum
Aluminum Alloy Microstructure Properties
article

Effect of Homogenization Cycle on Precipitation of Dispersoids and Abnormal Grain Growth in an Al-Mg-Si Alloy

Manu Saxena, Sumit Kumar Gahlyan, Vivek Srivastava, Shavi Agrawal, Butchi Bharadwaj, Pankaj Shivaji Wanjari
article en

Abstract

AA6xxx alloys are used for various automotive and architectural applications where microstructural characteristics are critical to have acceptable final properties. Abnormal Grain Growth (AGG) in these alloys, industrially termed as Peripheral Coarse Grain (PCG) is undesirable and Mn, Cr based non-coherent dispersoids are used to control the extent of PCG. Homogenization soaking temperature and time along with heating rates determine the size, distribution with grains and volume fraction of these dispersoids. In this study the heating rates are varied in lab and industrial setting to assess the effect of aforementioned dispersoid features using SEM and digital microscopy. It is found that higher heating rates lead to coarser and lower area fraction of dispersoids which finally results in markedly large PCG in industrial extrusion. Observed dispersoid features were described based on basic kinetics and Thermo-Calc TM predicted trends of micro-segregation, fraction of dispersoids and fraction of potential nucleating sites (β’-Mg 2 Si) of dispersoids. A static recrystallization model was used to calculate the driving and retarding pressures based on substructural (EBSD analysis) and dispersoid features (SEM+ image analysis). The predicted recrystallisation response and PCG grain size was in close agreement with the observed values. This study highlights the significance of homogenization heating rates in addition to soaking time and temperature for PCG control.

Materials science forumVol. 1130
Indian Institute of Science
Openalex Percentile: Top 70%
Aluminum Alloy Microstructure Properties
AI Navigator

Ask Laika to Summarize, Analyze, and Connect papers live on the map.

Summarize Papers & Methodologies

Extract key findings, datasets, and comparative methods across publications.

Benchmark Rankings & Visual Analytics

Rank top research institutions, authors, funders, topics, and journals by Field-Weighted Citation Impact (FWCI) and paper volume with instant charts.

Connect Distant Disciplines

Bridge topological clusters on the map to find hidden collaborative intersections.