Extending the Transient Plane Source Scanning method for determining the specific heat capacity of low thermal conductivity materials through a numerical study

In contrast to the conventional Transient Plane Source (TPS) method, the Transient Plane Source Scanning (TPSS) technique allows for the direct determination of the specific heat capacity and requires the use of a specially designed sample holder for accurate measurements. While this method correctly determines the specific heat capacity of samples with moderate and high thermal conductivity, it tends to underestimate the values for those with low thermal conductivity. This paper demonstrates that the underestimated specific heat capacity results from heat loss during the measurement process. To precisely quantify the heat loss, a numerical model based on the finite element method was developed, with key material properties tuned based on measurement data. This model can closely describe the curve of measured thermal response, thereby enabling the precise determination of the specific heat capacity. Consequently, this study introduces a novel approach that incorporates numerical simulation to enhance TPSS measurements of poorly conducting samples, providing a reliable alternative for determining the specific heat capacity. • A promising alternative for measuring specific heat capacity was greatly improved. • Parameter estimation based on numerical study enhances the data analysis. • Heat loss plays a critical role in the measurement. • Good agreement with reference data was achieved, with differences less than 4.4%.

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Publication Details

Journal
Thermochimica Acta
Published
2024-10-28
DOI
https://doi.org/10.1016/j.tca.2024.179883
Citations
4
Primary Topic
Phase Change Materials Research
Type
article
Field-Weighted Citation Impact
0.85

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article

Extending the Transient Plane Source Scanning method for determining the specific heat capacity of low thermal conductivity materials through a numerical study

Christian Müller, Zijin Zeng, Besira Mihiretie
4 citations
Thermochimica Acta
Phase Change Materials Research
0.85
article

Extending the Transient Plane Source Scanning method for determining the specific heat capacity of low thermal conductivity materials through a numerical study

Christian Müller, Zijin Zeng, Besira Mihiretie
article en
4 citations

Abstract

In contrast to the conventional Transient Plane Source (TPS) method, the Transient Plane Source Scanning (TPSS) technique allows for the direct determination of the specific heat capacity and requires the use of a specially designed sample holder for accurate measurements. While this method correctly determines the specific heat capacity of samples with moderate and high thermal conductivity, it tends to underestimate the values for those with low thermal conductivity. This paper demonstrates that the underestimated specific heat capacity results from heat loss during the measurement process. To precisely quantify the heat loss, a numerical model based on the finite element method was developed, with key material properties tuned based on measurement data. This model can closely describe the curve of measured thermal response, thereby enabling the precise determination of the specific heat capacity. Consequently, this study introduces a novel approach that incorporates numerical simulation to enhance TPSS measurements of poorly conducting samples, providing a reliable alternative for determining the specific heat capacity. • A promising alternative for measuring specific heat capacity was greatly improved. • Parameter estimation based on numerical study enhances the data analysis. • Heat loss plays a critical role in the measurement. • Good agreement with reference data was achieved, with differences less than 4.4%.

Thermochimica ActaVol. 742
Hot Disk (Sweden) (SE), Chalmers University of Technology (SE)
European Commission, Horizon 2020 Framework Programme, Horizon 2020, H2020 Marie Skłodowska-Curie Actions
Affordable and clean energy
Openalex Percentile: Top 30%
Phase Change Materials Research
0.85
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Extending the Transient Plane Source Scanning method for determining the specific heat capacity of low thermal conductivity materials through a numerical study — Christian Müller, Zijin Zeng, et al. · Thermochimica Acta (2024) | TGRS Research Map | TGRS