Altering microstructure and enhancing mechanical properties during direct energy deposition of Ti-6Al-4V via in-process laser heat treatments

In-process laser-based heat treatments (LHTs) during additive manufacturing are explored as an alternative to post-process heat treatments such as annealing, to alter the microstructure and mechanical properties of Ti-6Al-4V. Three samples were manufactured via laser-based direct energy deposition with the laser operating at 300 W. One as-built sample without any LHTs served as the reference sample. For the remaining two, each deposited layer was subjected to an additional LHT just after its deposition; LHTs were performed at 100 W for one (LHT100) and 300 W for the other (LHT300) without powder addition. LHT100 showed an overall improvement in the strength/ductility trade-off. Whereas LHT300 resulted in a lower strength but a much higher ductility and toughness than the other two samples. Synchrotron X-ray diffraction analysis of as-built samples revealed an insignificant difference in the bcc (β) and combined hcp (martensite alpha', diffusively formed alpha_d and massively transformed alpha_m) phases between different samples. However, scanning electron microscopy uncovered a significant effect of LHTs in varying the fractions of different hcp phases between samples, which is the main cause behind mechanical property differences. These results demonstrate the significant potential of in-process LHTs to tailor alloy microstructures for achieving desired mechanical properties.

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Publication Details

Journal
Materials & Design
Published
2025-04-29
DOI
https://doi.org/10.1016/j.matdes.2025.113997
Citations
2
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
1.43

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article

Altering microstructure and enhancing mechanical properties during direct energy deposition of Ti-6Al-4V via in-process laser heat treatments

Kouider Abdellah Abdesselam, Manas Vijay Upadhyay, Steve Gaudez, Maxime Vallet et al.
2 citations
Materials & Design
Additive Manufacturing Materials and Processes
1.43
article

Altering microstructure and enhancing mechanical properties during direct energy deposition of Ti-6Al-4V via in-process laser heat treatments

Kouider Abdellah Abdesselam, Manas Vijay Upadhyay, Steve Gaudez, Maxime Vallet, Louis Cornet, S. Van Petegem, V. Honkimäki, Simon Hallais
article en
2 citations

Abstract

In-process laser-based heat treatments (LHTs) during additive manufacturing are explored as an alternative to post-process heat treatments such as annealing, to alter the microstructure and mechanical properties of Ti-6Al-4V. Three samples were manufactured via laser-based direct energy deposition with the laser operating at 300 W. One as-built sample without any LHTs served as the reference sample. For the remaining two, each deposited layer was subjected to an additional LHT just after its deposition; LHTs were performed at 100 W for one (LHT100) and 300 W for the other (LHT300) without powder addition. LHT100 showed an overall improvement in the strength/ductility trade-off. Whereas LHT300 resulted in a lower strength but a much higher ductility and toughness than the other two samples. Synchrotron X-ray diffraction analysis of as-built samples revealed an insignificant difference in the bcc (β) and combined hcp (martensite alpha', diffusively formed alpha_d and massively transformed alpha_m) phases between different samples. However, scanning electron microscopy uncovered a significant effect of LHTs in varying the fractions of different hcp phases between samples, which is the main cause behind mechanical property differences. These results demonstrate the significant potential of in-process LHTs to tailor alloy microstructures for achieving desired mechanical properties.

Materials & DesignVol. 254
European Synchrotron Radiation Facility (FR), Paul Scherrer Institute (CH), Laboratoire Mécanique des Solides (FR), CentraleSupélec (FR), Laboratoire de Mécanique Paris-Saclay (FR), Laboratoire Structures, Propriétés et Modélisation des Solides (FR)
European Commission, European Synchrotron Radiation Facility, European Research Council, Horizon 2020, H2020 European Research Council
Affordable and clean energy
Openalex Percentile: Top 23%
Additive Manufacturing Materials and Processes
1.43
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