Investigation of the Effect of Milling Time on Elemental Powders of Oxi‐Reduction Nickel and Hydrogenation–Dehydrogenation Titanium

Mechanical alloying (MA) is widely applied in the synthesis of blended elemental or prealloyed powders. This work evaluates the effect of milling time on elemental nickel and titanium powders produced by oxi‐reduction and the hydrogenation–dehydrogenation process, respectively. The powders are characterized by scanning electron microscopy, X‐ray diffraction, particle size, powder yield, and differential scanning calorimetry. It is observed that increasing the milling time promotes the formation of a structure composed of thin lamellae of nickel and titanium, which results in the beneficial effect of lowering the temperature for the formation of the intermetallic of the Ni–Ti system and in the powder yield achieved. The reduction of milling time in the MA process of NiTi alloys enhances technological efficiency by decreasing their overall processing time.

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Publication Details

Journal
Advanced Engineering Materials
Published
2024-10-25
DOI
https://doi.org/10.1002/adem.202401031
Primary Topic
Advanced materials and composites
Type
article
Field-Weighted Citation Impact
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article

Investigation of the Effect of Milling Time on Elemental Powders of Oxi‐Reduction Nickel and Hydrogenation–Dehydrogenation Titanium

Rebeca Vieira de Oliveira, Patrícia Freitas Rodrigues, Andersan dos Santos Paula, Filipe Neves et al.
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Advanced Engineering Materials
Advanced materials and composites
article

Investigation of the Effect of Milling Time on Elemental Powders of Oxi‐Reduction Nickel and Hydrogenation–Dehydrogenation Titanium

Rebeca Vieira de Oliveira, Patrícia Freitas Rodrigues, Andersan dos Santos Paula, Filipe Neves, Naiara Vieira Le Sénèchal, Rodolfo da Silva Teixeira, Bruno Xavier de Freitas, Mônica Aline Magalhães Gurgel
article en

Abstract

Mechanical alloying (MA) is widely applied in the synthesis of blended elemental or prealloyed powders. This work evaluates the effect of milling time on elemental nickel and titanium powders produced by oxi‐reduction and the hydrogenation–dehydrogenation process, respectively. The powders are characterized by scanning electron microscopy, X‐ray diffraction, particle size, powder yield, and differential scanning calorimetry. It is observed that increasing the milling time promotes the formation of a structure composed of thin lamellae of nickel and titanium, which results in the beneficial effect of lowering the temperature for the formation of the intermetallic of the Ni–Ti system and in the powder yield achieved. The reduction of milling time in the MA process of NiTi alloys enhances technological efficiency by decreasing their overall processing time.

Advanced Engineering MaterialsVol. 27(6)
Centre National de la Recherche Scientifique (FR), Université Paris-Saclay (FR), Instituto Nacional de Metrologia, Qualidade e Tecnologia (BR), Military Institute of Engineering (BR), National Laboratory of Energy and Geology (PT), CentraleSupélec (FR), University of Coimbra (PT), Universidade Federal de Itajubá (BR)
Fundo Regional para a Ciência e Tecnologia, Fundação para a Ciência e a Tecnologia
Industry, innovation and infrastructure
Openalex Percentile: Top 81%
Advanced materials and composites
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