SEM-DIC characterization of the damage mechanism of an AlSi10Fe0.7 casting alloy on the microstructure scale

Various brittle phases are present in commercial cast aluminum alloys, which strongly influence their mechanical behavior. Among these, silicon precipitates are nearly omnipresent, as Si is a common alloying element. In secondary alloys, usually Fe-containing phases cannot be avoided, and they tend to degrade the mechanical properties. The interaction between the silicon phase and the failure-critical intermetallic phase in the Al-Si-Fe phase system (β- Al 5 FeSi ) is studied in this paper in high resolution. A model alloy AlSi10Fe0.7 was defined, which is composed of a large grain Al-matrix, Si-precipitates and the plate-like β- Al 5 FeSi phase. The goal of the study was to identify “hot spots” in the microstructure from which cracks may initiate under mechanical loading. The main tool was a deformation analysis via digital image correlation in the SEM (SEM-DIC). This allows the identification and tracking of developing strain localizations at different potential crack initiation sites with a high resolution as well as capturing an overview over the whole specimen. An adapted frame averaging script minimized measurement errors induced by drift. The SEM-DIC results show that the deformation field is governed by the elastic incompatibility of the microstructural constituents. Crack initiation occurs because of the detachment of the Si + β- Al 5 FeSi phase boundary. Cracks then cross the phase boundary and propagate along twin boundaries in the β- Al 5 FeSi phase. Final failure is caused by linking fractured brittle plate-like particles. • A deformation analysis of a secondary AlSi casting alloy was concluded via SEM-DIC. • The interaction between the brittle silicon phase and the β- Al 5 FeSi phase was studied. • Crack initiation occurs because of the detachment of the Si + β- Al 5 FeSi phase boundary. • It is indicated that the fracture of the β-platelet is governed by the crack's propagation between altering twin boundaries.

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Publication Details

Journal
Materials Characterization
Published
2024-10-20
DOI
https://doi.org/10.1016/j.matchar.2024.114478
Citations
1
Primary Topic
Aluminum Alloy Microstructure Properties
Type
article
Field-Weighted Citation Impact
1.30
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article

SEM-DIC characterization of the damage mechanism of an AlSi10Fe0.7 casting alloy on the microstructure scale

H. Meckbach, T. Ickler, Martin Fehlbier, F. Zeismann et al.
1 citations
Materials Characterization
Aluminum Alloy Microstructure Properties
1.30
article

SEM-DIC characterization of the damage mechanism of an AlSi10Fe0.7 casting alloy on the microstructure scale

H. Meckbach, T. Ickler, Martin Fehlbier, F. Zeismann, Daniel Jüngst, A. Brückner‐Foit
article en
1 citations

Abstract

Various brittle phases are present in commercial cast aluminum alloys, which strongly influence their mechanical behavior. Among these, silicon precipitates are nearly omnipresent, as Si is a common alloying element. In secondary alloys, usually Fe-containing phases cannot be avoided, and they tend to degrade the mechanical properties. The interaction between the silicon phase and the failure-critical intermetallic phase in the Al-Si-Fe phase system (β- Al 5 FeSi ) is studied in this paper in high resolution. A model alloy AlSi10Fe0.7 was defined, which is composed of a large grain Al-matrix, Si-precipitates and the plate-like β- Al 5 FeSi phase. The goal of the study was to identify “hot spots” in the microstructure from which cracks may initiate under mechanical loading. The main tool was a deformation analysis via digital image correlation in the SEM (SEM-DIC). This allows the identification and tracking of developing strain localizations at different potential crack initiation sites with a high resolution as well as capturing an overview over the whole specimen. An adapted frame averaging script minimized measurement errors induced by drift. The SEM-DIC results show that the deformation field is governed by the elastic incompatibility of the microstructural constituents. Crack initiation occurs because of the detachment of the Si + β- Al 5 FeSi phase boundary. Cracks then cross the phase boundary and propagate along twin boundaries in the β- Al 5 FeSi phase. Final failure is caused by linking fractured brittle plate-like particles. • A deformation analysis of a secondary AlSi casting alloy was concluded via SEM-DIC. • The interaction between the brittle silicon phase and the β- Al 5 FeSi phase was studied. • Crack initiation occurs because of the detachment of the Si + β- Al 5 FeSi phase boundary. • It is indicated that the fracture of the β-platelet is governed by the crack's propagation between altering twin boundaries.

Materials CharacterizationVol. 218
University of Kassel (DE)
Openalex Percentile: Top 12%
Aluminum Alloy Microstructure Properties
1.30
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