Synthesis of ZnO NWs via Thermal Evaporation Technique

Zinc oxide nanowires ZnONWs were successfully synthesized on glass slides. The synthesis was conducted firstly by the deposition of 12 µm a thin film of Zn metal by thermal evaporation. Secondly,the coated film was annealed at a temperature of 600 ºC in air for four hours to grow the ZnO nanowires. It have been observed that the produced nanowires were grown in a vertical orientation and having a high density, very long, and a minimal aspect ratio. The crystal structure and morphology of ZnO nanowires were investigated with X-ray diffraction (XRD) and scanning electron microscopy (SEM). The UV-visible spectrophotometer was also used to calculate the optical parameters from the absorption spectrum and show a band gap energy around 3.25 eV. The crystal structure of the material was revealed to be polycrystalline with a preferred orientation in the direction of [101]. Small average crystallite size was calculated about 17nm The wires can be measured to have a length of around 10 µm with diameters ranging from 50 to 100 nm. This could be used for gas sensor applications. In addition, this ZnONWs structure has a maximum transmittance (100%) which can be a good candidate for many optoelectronic apllications.

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Publication Details

Journal
Iraqi Journal of Industrial Research
Published
2024-10-20
DOI
https://doi.org/10.53523/ijoirvol11i2id421
Primary Topic
ZnO doping and properties
Type
article
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article

Synthesis of ZnO NWs via Thermal Evaporation Technique

Waqas Khalid, Abdulqader D. Faisal, Ali A. Aljubouri
Iraqi Journal of Industrial Research
ZnO doping and properties
article

Synthesis of ZnO NWs via Thermal Evaporation Technique

Waqas Khalid, Abdulqader D. Faisal, Ali A. Aljubouri
article en

Abstract

Zinc oxide nanowires ZnONWs were successfully synthesized on glass slides. The synthesis was conducted firstly by the deposition of 12 µm a thin film of Zn metal by thermal evaporation. Secondly,the coated film was annealed at a temperature of 600 ºC in air for four hours to grow the ZnO nanowires. It have been observed that the produced nanowires were grown in a vertical orientation and having a high density, very long, and a minimal aspect ratio. The crystal structure and morphology of ZnO nanowires were investigated with X-ray diffraction (XRD) and scanning electron microscopy (SEM). The UV-visible spectrophotometer was also used to calculate the optical parameters from the absorption spectrum and show a band gap energy around 3.25 eV. The crystal structure of the material was revealed to be polycrystalline with a preferred orientation in the direction of [101]. Small average crystallite size was calculated about 17nm The wires can be measured to have a length of around 10 µm with diameters ranging from 50 to 100 nm. This could be used for gas sensor applications. In addition, this ZnONWs structure has a maximum transmittance (100%) which can be a good candidate for many optoelectronic apllications.

Iraqi Journal of Industrial ResearchVol. 11(2)
University of Technology - Iraq (IQ), Universitas Ibn Khaldun Bogor (ID)
Openalex Percentile: Top 89%
ZnO doping and properties
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Synthesis of ZnO NWs via Thermal Evaporation Technique — Waqas Khalid, Abdulqader D. Faisal, et al. · Iraqi Journal of Industrial Research (2024) | TGRS Research Map | TGRS