Fourier Transform Infrared Spectroscopy (FTIR) for identification of sugar adulterants in mulberry molasses (pekmez)

Fourier Transform Infrared Spectroscopy (FTIR) and chemometrics were successfully used in this research in conjunction with the Attenuated Total Reflectance (ATR) technique to determine bulberry molasses (MM) canesugar adulteration. Mulberry molasses was adultered by incorporating two fructose syrups (FS), one glucose syrup (GS), one sucrose syrup (SS), and two specific high fructose corn syrups (HFCS). Calibration sets were developed for mulberry molasses by spiking sugar syrups. The actual percentage of adulteration linked to FTIR predicted results by partial least square (PLS). The preferred spectral range was 1184-944 cm-1 for prediction of adulteration levels of F20, F30, HFCS50, HFCS55 and 1090-950 cm-1 for sucrose. This method was employed to distinguish between mulberry molasses and adulterated samples. According to the findings, the FTIR technique is an accurate and affordable method that can rapidly detect sugar adulteration in mulberry molasses.

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Publication Details

Journal
Latin American Applied Research - An international journal
Published
2024-10-07
DOI
https://doi.org/10.52292/j.laar.2024.3318
Primary Topic
Food Quality and Safety Studies
Type
article
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article

Fourier Transform Infrared Spectroscopy (FTIR) for identification of sugar adulterants in mulberry molasses (pekmez)

Muhammed Zeki Durak, Nur Çebi, Mehmet Fatih Cengiz, Fidan Özge
Latin American Applied Research - An international journal
Food Quality and Safety Studies
article

Fourier Transform Infrared Spectroscopy (FTIR) for identification of sugar adulterants in mulberry molasses (pekmez)

Muhammed Zeki Durak, Nur Çebi, Mehmet Fatih Cengiz, Fidan Özge
article en

Abstract

Fourier Transform Infrared Spectroscopy (FTIR) and chemometrics were successfully used in this research in conjunction with the Attenuated Total Reflectance (ATR) technique to determine bulberry molasses (MM) canesugar adulteration. Mulberry molasses was adultered by incorporating two fructose syrups (FS), one glucose syrup (GS), one sucrose syrup (SS), and two specific high fructose corn syrups (HFCS). Calibration sets were developed for mulberry molasses by spiking sugar syrups. The actual percentage of adulteration linked to FTIR predicted results by partial least square (PLS). The preferred spectral range was 1184-944 cm-1 for prediction of adulteration levels of F20, F30, HFCS50, HFCS55 and 1090-950 cm-1 for sucrose. This method was employed to distinguish between mulberry molasses and adulterated samples. According to the findings, the FTIR technique is an accurate and affordable method that can rapidly detect sugar adulteration in mulberry molasses.

Latin American Applied Research - An international journalVol. 54(4)
Ordu University (TR)
Openalex Percentile: Top 78%
Food Quality and Safety Studies
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