Soft X-ray chemically sensitive ptychographic imaging of 3D nano-objects

The results of a soft X-ray chemically sensitive ptychographic imaging of non-planar nanoscale 3D objects - atom probe tomography tips, with resolution down to 12 nm at 800 eV using scanning X-ray microscope at the electron storage ring BESSY II are presented. We validate that this approach can be used to determine the tip (emitter) shape, and to resolve inner nano-scale structures as relevant for semiconductor applications and even for quantitative chemical composition analysis. Imaging of buried interfaces with below 30 nm resolution is demonstrated. This work might pave the way for contactless, ptychographic in-situ characterization of APT tips with tabletop coherent EUV sources.

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Publication Details

Journal
Optics Express
Published
2024-10-10
DOI
https://doi.org/10.1364/oe.535314
Citations
4
Primary Topic
Advanced X-ray Imaging Techniques
Type
article
Field-Weighted Citation Impact
2.43

Funders

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article

Soft X-ray chemically sensitive ptychographic imaging of 3D nano-objects

Igor A. Makhotkin, Lars Loetgering, P.A.W. van der Heide, Victor Soltwisch et al.
4 citations
Optics Express
Advanced X-ray Imaging Techniques
2.43
article

Soft X-ray chemically sensitive ptychographic imaging of 3D nano-objects

Igor A. Makhotkin, Lars Loetgering, P.A.W. van der Heide, Victor Soltwisch, Claudia Fleischmann, Jeroen E. Scheerder, V. V. Krasnov
article en
4 citations

Abstract

The results of a soft X-ray chemically sensitive ptychographic imaging of non-planar nanoscale 3D objects - atom probe tomography tips, with resolution down to 12 nm at 800 eV using scanning X-ray microscope at the electron storage ring BESSY II are presented. We validate that this approach can be used to determine the tip (emitter) shape, and to resolve inner nano-scale structures as relevant for semiconductor applications and even for quantitative chemical composition analysis. Imaging of buried interfaces with below 30 nm resolution is demonstrated. This work might pave the way for contactless, ptychographic in-situ characterization of APT tips with tabletop coherent EUV sources.

Optics ExpressVol. 32(25)
Helmholtz Institute Jena (DE), Laboratoire de physique des Solides (FR), Polish Botanical Society (PL), Carl Zeiss (United States) (US), Friedrich Schiller University Jena (DE), University of Twente (NL)
Fonds Wetenschappelijk Onderzoek
Openalex Percentile: Top 11%
Advanced X-ray Imaging Techniques
2.43
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Soft X-ray chemically sensitive ptychographic imaging of 3D nano-objects — Igor A. Makhotkin, Lars Loetgering, et al. · Optics Express (2024) | TGRS Research Map | TGRS