On the effect of energy input on microstructure evolution and mechanical properties of laser beam powder bed fusion processed Ti-27Nb-6Ta biomedical alloy

Additive manufacturing of pre-alloyed Ti-27Nb-6Ta powder by laser beam powder bed fusion (PBF-LB/M) employing a wide range of processing parameters is reported. An in-depth microstructure analysis along the whole process chain from powder feedstock material to additively manufactured bulk structures was conducted employing scanning electron microscopy (SEM) as well as X-ray and high-energy synchrotron diffraction. It is shown that near-fully dense parts (≥ 99.96%) with β+α’’ dual-phase microstructure and very homogenous element distribution are obtained in a large process window. In particular, a considerable influence of the energy input during PBF-LB/M on the solidification microstructure, i.e. phase composition and texture, is found. With increasing energy per unit area (E A ) values both an increase in the volume fraction of the bcc β-phase and more pronounced texture components are seen. Furthermore, the mechanical behavior was evaluated under monotonic tensile loading. The PBF-LB/M processed Ti-27Nb-6Ta structures feature good mechanical properties with ultimate tensile strength (UTS) and strain to failure values of up to 768 MPa and 33.8 %, respectively. Due to the strong impact of the energy input during additive manufacturing on the microstructure evolution, however, a significant inverse strength-ductility behavior is observed. While UTS clearly decreases with increasing E A values, strain to failure increases at the same time. The underlying relationships between processing (energy input), microstructure and mechanical properties are explored and rationalized. • Additive manufacturing (AM) of pre-alloyed Ti-Nb-Ta powder by laser beam powder bed fusion (PBF-LB/M). • Chemically homogenous AM structures with near full density in a wide range of processing parameters. • Energy input during processing allows to tailor microstructure, phase constitution and mechanical properties of as-built parts. • The findings presented establish pathways for direct microstructure design in envisaged implant applications.

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Publication Details

Journal
Materials Science and Engineering A
Published
2024-10-09
DOI
https://doi.org/10.1016/j.msea.2024.147363
Citations
1
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
0.21

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On the effect of energy input on microstructure evolution and mechanical properties of laser beam powder bed fusion processed Ti-27Nb-6Ta biomedical alloy

Anna Engelhardt, Thomas Niendorf, Melanie Stenzel, Jan Johannsen et al.
1 citations
Materials Science and Engineering A
Additive Manufacturing Materials and Processes
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article

On the effect of energy input on microstructure evolution and mechanical properties of laser beam powder bed fusion processed Ti-27Nb-6Ta biomedical alloy

Anna Engelhardt, Thomas Niendorf, Melanie Stenzel, Jan Johannsen, Markus Weinmann, A. Bolender, C. Lauhoff
article en
1 citations

Abstract

Additive manufacturing of pre-alloyed Ti-27Nb-6Ta powder by laser beam powder bed fusion (PBF-LB/M) employing a wide range of processing parameters is reported. An in-depth microstructure analysis along the whole process chain from powder feedstock material to additively manufactured bulk structures was conducted employing scanning electron microscopy (SEM) as well as X-ray and high-energy synchrotron diffraction. It is shown that near-fully dense parts (≥ 99.96%) with β+α’’ dual-phase microstructure and very homogenous element distribution are obtained in a large process window. In particular, a considerable influence of the energy input during PBF-LB/M on the solidification microstructure, i.e. phase composition and texture, is found. With increasing energy per unit area (E A ) values both an increase in the volume fraction of the bcc β-phase and more pronounced texture components are seen. Furthermore, the mechanical behavior was evaluated under monotonic tensile loading. The PBF-LB/M processed Ti-27Nb-6Ta structures feature good mechanical properties with ultimate tensile strength (UTS) and strain to failure values of up to 768 MPa and 33.8 %, respectively. Due to the strong impact of the energy input during additive manufacturing on the microstructure evolution, however, a significant inverse strength-ductility behavior is observed. While UTS clearly decreases with increasing E A values, strain to failure increases at the same time. The underlying relationships between processing (energy input), microstructure and mechanical properties are explored and rationalized. • Additive manufacturing (AM) of pre-alloyed Ti-Nb-Ta powder by laser beam powder bed fusion (PBF-LB/M). • Chemically homogenous AM structures with near full density in a wide range of processing parameters. • Energy input during processing allows to tailor microstructure, phase constitution and mechanical properties of as-built parts. • The findings presented establish pathways for direct microstructure design in envisaged implant applications.

Materials Science and Engineering AVol. 918
University of Kassel (DE), Gobierno de Canarias (ES), Fraunhofer Research Institution for Additive Manufacturing Technologies IAPT (DE)
Bundesministerium für Bildung und Forschung, Universität Kassel
Affordable and clean energy
Openalex Percentile: Top 51%
Additive Manufacturing Materials and Processes
0.21
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