Fatigue mechanisms at 450°C of a highly twined (>70%) and HIP-densified IN718 superalloy additively manufactured by laser beam powder bed fusion

• High twin fraction (>70 %) in PBF-LB IN718 from supersolvus treatments with HIP . • Fatigue with low scatter dominated by grain, as pores and brittle phases minimized. • The twin effect is limited at low △K but causes cracking in high-△K conditions. • Higher angles (60⁰) in twins than HAGBs (mostly 30–40⁰) resist fatigue propagation. • Randomly oriented twins likely provided net strengthening effects . Fatigue resistance at elevated temperatures is crucial for certifying aerospace structures additively manufactured by the laser beam powder bed fusion (PBF-LB) method with IN718 superalloy. This study employed a multi-step, supersolvus heat treatment process with hot isostatic pressing (HIP), called RHSA, to minimize pores and brittle phases. Stress intensity factor (△K) calculations using data from X-ray computed tomography and shape factors referencing finite element analysis (FEA) studies confirmed the suppression of △K below the threshold of conventional IN718 (∼5 MPa√m), shifting fatigue behavior to grain-structure-dominated. Despite a very high twin boundary (TB) fraction (>70%), fatigue tests at 450°C and R = 0.1 demonstrated low scatter. Slip trace analysis and high-resolution electron backscatter diffraction (EBSD) revealed that TB-induced strain concentration became prominent only at high △K, causing cracking at 45⁰ to the loading direction. The randomly oriented TBs with higher angles (60⁰) compared to high-angle grain boundaries (HAGBs) (30–40⁰) likely enhanced slip resistance and provided a net strengthening effect, which can explain the lower-than-average TB% along fracture paths. These insights suggest that a high TB fraction is not detrimental if fatigue stress is not excessive, alleviating concerns about annealing twins during defect minimization in AM IN718, allowing novel processes to improve fatigue resistance in PBF-LB IN718.

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Publication Details

Journal
International Journal of Fatigue
Published
2024-10-03
DOI
https://doi.org/10.1016/j.ijfatigue.2024.108629
Citations
8
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
1.70
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article

Fatigue mechanisms at 450°C of a highly twined (>70%) and HIP-densified IN718 superalloy additively manufactured by laser beam powder bed fusion

Amberlee S. Haselhuhn, Sammy Tin, Andrew Wessman, Anthony Koumpias et al.
8 citations
International Journal of Fatigue
Additive Manufacturing Materials and Processes
1.70
article

Fatigue mechanisms at 450°C of a highly twined (>70%) and HIP-densified IN718 superalloy additively manufactured by laser beam powder bed fusion

Amberlee S. Haselhuhn, Sammy Tin, Andrew Wessman, Anthony Koumpias, Alexis Loustaunau, Marcus C. Lam, Carla Michelle Colon Cruz
article en
8 citations

Abstract

• High twin fraction (>70 %) in PBF-LB IN718 from supersolvus treatments with HIP . • Fatigue with low scatter dominated by grain, as pores and brittle phases minimized. • The twin effect is limited at low △K but causes cracking in high-△K conditions. • Higher angles (60⁰) in twins than HAGBs (mostly 30–40⁰) resist fatigue propagation. • Randomly oriented twins likely provided net strengthening effects . Fatigue resistance at elevated temperatures is crucial for certifying aerospace structures additively manufactured by the laser beam powder bed fusion (PBF-LB) method with IN718 superalloy. This study employed a multi-step, supersolvus heat treatment process with hot isostatic pressing (HIP), called RHSA, to minimize pores and brittle phases. Stress intensity factor (△K) calculations using data from X-ray computed tomography and shape factors referencing finite element analysis (FEA) studies confirmed the suppression of △K below the threshold of conventional IN718 (∼5 MPa√m), shifting fatigue behavior to grain-structure-dominated. Despite a very high twin boundary (TB) fraction (>70%), fatigue tests at 450°C and R = 0.1 demonstrated low scatter. Slip trace analysis and high-resolution electron backscatter diffraction (EBSD) revealed that TB-induced strain concentration became prominent only at high △K, causing cracking at 45⁰ to the loading direction. The randomly oriented TBs with higher angles (60⁰) compared to high-angle grain boundaries (HAGBs) (30–40⁰) likely enhanced slip resistance and provided a net strengthening effect, which can explain the lower-than-average TB% along fracture paths. These insights suggest that a high TB fraction is not detrimental if fatigue stress is not excessive, alleviating concerns about annealing twins during defect minimization in AM IN718, allowing novel processes to improve fatigue resistance in PBF-LB IN718.

International Journal of FatigueVol. 190
University of Arizona (US), Detroit R&D (United States) (US)
Openalex Percentile: Top 17%
Additive Manufacturing Materials and Processes
1.70
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