Optimization of Electroless Plating Solution Parameter for Coating PETG Electrode with Copper using Design of Experiment (DOE)

In the study, an attempt was made to electrolessly plate copper onto PETG plastics that aren't conductors. Three manipulating factors, i.e. volume of copper sulphate and sulphuric acid (A), volume of sulphuric acid (B), and mass of copper sulphate (C), were selected and carried out using Taguchi method with three levels to examine their interactions and effects on the responses, including plating thickness, and electrical resistance. The Design Expert 13 software creates a total of nine runs with a single centre point. Three days were spent submerging every electroplated sample part in a different bath solution concentration. The resistance of the metalized PETG component was measured in the meantime using a digital multi-meter. The Cu-deposited PETG was analysed and measured using scanning electron microscopy (SEM). The ideal situation was identified as having 10 possibilities for achieving the goal, based on interaction effects. According to the results of the experiment, run number 3 provides the ideal solution parameter for copper deposition metallization. For the lowest electrical resistance of 0.64 ohm and the highest plating thickness value of 211.49 m, these runs yield the best ideal results. Because each factor reacts to a response individually, the Analysis of Variance (ANOVA) demonstrates that there are little interactions between the factors and responses. The lowest electrical resistance and highest plating thickness values are obtained with the best chemical composition parameter choices.

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Publication Details

Journal
Journal of Advanced Research in Applied Mechanics
Published
2024-10-02
DOI
https://doi.org/10.37934/aram.125.1.113
Primary Topic
Electrodeposition and Electroless Coatings
Type
article
Field-Weighted Citation Impact
0.00

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article

Optimization of Electroless Plating Solution Parameter for Coating PETG Electrode with Copper using Design of Experiment (DOE)

Sharifah Adzila Syed Abu Bakar, Reazul Haq Abdul Haq, Yashvir Singh, J. Hoffmann et al.
Journal of Advanced Research in Applied Mechanics
Electrodeposition and Electroless Coatings
article

Optimization of Electroless Plating Solution Parameter for Coating PETG Electrode with Copper using Design of Experiment (DOE)

Sharifah Adzila Syed Abu Bakar, Reazul Haq Abdul Haq, Yashvir Singh, J. Hoffmann, Mohd Fahrul Hassan, Mohammad Fahmi Abdul Ghafir, Fong Mun Kit
article en

Abstract

In the study, an attempt was made to electrolessly plate copper onto PETG plastics that aren't conductors. Three manipulating factors, i.e. volume of copper sulphate and sulphuric acid (A), volume of sulphuric acid (B), and mass of copper sulphate (C), were selected and carried out using Taguchi method with three levels to examine their interactions and effects on the responses, including plating thickness, and electrical resistance. The Design Expert 13 software creates a total of nine runs with a single centre point. Three days were spent submerging every electroplated sample part in a different bath solution concentration. The resistance of the metalized PETG component was measured in the meantime using a digital multi-meter. The Cu-deposited PETG was analysed and measured using scanning electron microscopy (SEM). The ideal situation was identified as having 10 possibilities for achieving the goal, based on interaction effects. According to the results of the experiment, run number 3 provides the ideal solution parameter for copper deposition metallization. For the lowest electrical resistance of 0.64 ohm and the highest plating thickness value of 211.49 m, these runs yield the best ideal results. Because each factor reacts to a response individually, the Analysis of Variance (ANOVA) demonstrates that there are little interactions between the factors and responses. The lowest electrical resistance and highest plating thickness values are obtained with the best chemical composition parameter choices.

Journal of Advanced Research in Applied MechanicsVol. 125(1)
Osnabrück University (DE), Hochschule Osnabrück (DE), Graphic Era University (IN), Tun Hussein Onn University of Malaysia (MY)
Universiti Tun Hussein Onn Malaysia
Openalex Percentile: Top 86%
Electrodeposition and Electroless Coatings
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