Development of a one-pot synthesis of rGO in water by optimizing Tour’s method parameters

Since its first synthesis in 2004, graphene has been widely studied and several different synthesis methods has been developed. Solvent exfoliation of graphite and the reduction of graphene oxide previously obtained through graphite oxidation are the most employed. In this work, we exploited synthesis conditions of a method usually employed for obtaining graphene oxide (the Tour's method) for directly obtaining a very poorly oxidised material with characteristics like reduced graphene oxide. For the first time, a one-pot synthesis of reduced graphene oxide (rGO) is reported avoiding the use of a post-synthesis chemical or thermal reduction of the graphene oxide that requires further reagents, heat and time.

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Publication Details

Journal
Scientific Reports
Published
2024-09-27
DOI
https://doi.org/10.1038/s41598-024-73606-2
Citations
5
Primary Topic
Graphene research and applications
Type
article
Field-Weighted Citation Impact
0.59

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article

Development of a one-pot synthesis of rGO in water by optimizing Tour’s method parameters

Fabrizio Sordello, Rosangela Santalucia, Paul Mrkwitschka, Francesco Pellegrino et al.
5 citations
Scientific Reports
Graphene research and applications
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article

Development of a one-pot synthesis of rGO in water by optimizing Tour’s method parameters

Fabrizio Sordello, Rosangela Santalucia, Paul Mrkwitschka, Francesco Pellegrino, Vasile‐Dan Hodoroaba, Veno Kononenko, Jörg Radnik, Damjana Drobne, Andrea Mario Rossi, Sara Novak, K. Jurkschat, Eugenio Alladio, Loay Akmal Madbouly, Špela Saje
article en
5 citations

Abstract

Since its first synthesis in 2004, graphene has been widely studied and several different synthesis methods has been developed. Solvent exfoliation of graphite and the reduction of graphene oxide previously obtained through graphite oxidation are the most employed. In this work, we exploited synthesis conditions of a method usually employed for obtaining graphene oxide (the Tour's method) for directly obtaining a very poorly oxidised material with characteristics like reduced graphene oxide. For the first time, a one-pot synthesis of reduced graphene oxide (rGO) is reported avoiding the use of a post-synthesis chemical or thermal reduction of the graphene oxide that requires further reagents, heat and time.

Scientific ReportsVol. 14(1)
Federal Institute For Materials Research and Testing (DE), University of Ljubljana (SI), University of Oxford (GB), Oxford Medical Diagnostics (United Kingdom) (GB), University of Turin (IT)
Dipartimenti di Eccellenza, European Commission, Ministero dell’Istruzione, dell’Università e della Ricerca, Horizon 2020 Framework Programme
Clean water and sanitation
Openalex Percentile: Top 33%
Graphene research and applications
0.59
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